Title of Invention

A TWO-PHASE DISTRIBUTOR SYSTEM FOR DIRECTING VAPOR AND LIQUID DOWNWARDLY ACROSS THE SURFACE OF A FIXED BED OF SOLIDS

Abstract Abstract:- A description is given of a plant for heat treatment of lumpy material, such as limestone, other carbonate materials, cement raw materials, or the like. The plant comprises a preheating zone (1), a burning zone (3), and connecting means (20) which connect the material outlet (7) of the preheating zone to the materia! inlet (13) of the burning zone. A separating device (21) is provided as a part of the connecting means (20) and consists of a duct (21) through which a gas stream can be induced to flow from below and upwards. So, on entry into the separating duct (21) at the top of the duct, the preheated material will be dispersed in the counterflowing gas stream, whereby the material is divided into a fine fraction which suspended in the gas can be discharged via the discharge means (25) provided at the upper end of the duct, and a fall-through coarse fraction which in normal manner can be fed via a connecting means (20) to the material inlet (13) of the burning zone. PRICE: THIRTY RUPEES
Full Text



The present invention relates to a plant for heat treatment of lumpy material such as limestone, other carbonate minerals, cement raw materials, or the like, which plant comprises a preheating zone, preferably in the form of a shaft preheater, with at least one material inlet, at least one material outlet, at least one inlet for preheating gas, and at least one outlet for used preheating gas, in which preheating zone the material is preheated by means of hot preheating gas from which it is subsequently separated, a burning zone, e.g. in the form of a rotary kiln, v;ith material inlet and outlet, for burning the preheated material, connecting means which connect the material outlet of the preheating zone to the material inlet of the burning zone, and e separating device fitted in connectior: with the connecting means for separating the finest particles from, the preheated material .
When operating a plant of the aforementioned kind, the material leaving the preheating zone may contain a certain amount cf fine material being produced eitnei by decrepita¬tion of the marerial during the preheating, of lesulting from the material being exposed to wear o: dust from the burning zone which is drawn along up to the fireheating zone, subsequently settling there.
Ihere are primarily two reasons why it is desirable to minimize the amount of this fine material before the preheated material is fed to the kiln. One reason is that the fine material may have a disturbing effect on the kiln operation because of dust generation and coatings in the kiln and/or in exhaust gas ducts connected thereto. The second reason is that the amount of substances which are undesirable in the finished product, and which have the strongest tendency to stick to the finest material frac¬tions during the manufacturing process, can be reduced in this way.

As a case in point, it can be mentioned that the permis¬sible sulphur content in lime which is utilized in the steel-making industry is normally specified to be 0.03 to 0.05%. It follows that the sulphur content in the lime product depends on the amount of sulphur being fed to the kiln plant via the raw materials and the fuel. The sulphur content in raw materials may range from approximately 0 to 0.5%, while the sulphur content in fuel types such as oil and coal may be as high as 5%. In the majority of cases it will, therefore, be necessary to remove sulphur from the manufacturing process in order to meet the requirements which apply in terms of sulphur content in the finished product. This can be done by removing the finest material fractions, since, in relative terms, these fractions absorb the highest amount of sulphur because of their greater surface area.
A known method for removing the finest material consists of simple mechanical screening where the finest material is
) screened off by means of a sortinc grete :installed in the duct for feeding cf material to the . The disadvantage of using such a sortinc grate is, however, that clogging cf the grate will occur within a relatively short period of time, which entails that the grate loses its function. This
) occurs particularly in cases where the preheated feed material to the kiln is fine. Another disadvantage is the attendant risk of deformation of the grate due to the temperature between 650 and 900°C which prevails in this area.
)
It is the object of the present invention to provide a plant for heat treatment of lumpy material by means of which the aforementioned disadvantages are remedied.
5 This is achieved according to the invention by a plant of the kind mentioned in the introduction, and being charac¬terized in that the separating device is provided as a part



conjunction with the charactertics of the material, is the main determinant for the limit of separation between particle sizes which are entrained by the gas and the particle sizes which fall through. In order to incorporate into the plant a certain degree of flexibility both as regards the capability of handling different types of material and the ability to vary the limit of separation between the particles which entrained in the gas end up in the fine fraction and the fall-through particles which end up in the kiln, the plant may include means for regulating the gas velocity through the separating duct.
These means for regulating the gas velocity may comprise the fan which provides for the movement of the gas through the separating duct, particularly if the fan is not the same as that which is used to draw the exhaust gas through the plant. It is further preferred to use dampers for speed regulation.
The gas which is used for the separation process may theoretically be taken fror many different sources. It may be taken from the atmosphere as cold, atmospheric air, from the kiln as exhaust gas, from the exhaust gas duct of the preheater as exhaust gas used for preheating, or if a shaft preheater is used from this in the form of air used for cooling hereof. Hot excess air may also be used, for example the hot cooling air from a product cooler fitted after the kiln. Furthermore, the used separating gas may optionally be recirculated.
If the separating gas is taken as cold, atmospheric air it will exchange heat with the preheated material during the separation process and will be heated to a temperature of 450-650°C. The heat loss thereby incurred depends on this temperature and the amount of air taken in. However, a substantial reduction of the heat loss can be achieved by recirculating the air after a separation of the from the

separating duct entrained particles, and supplementing only with new atmospheric air to the extent necessary.
If the separating gas is taken as exhaust gas from the kiln, it may either be drawn up through the material feed duct, be taken from the smoke chamber of the kiln, or from the exhaust gas ducts which connect the smoke chamber to the preheater. The exhaust gas temperature will typically lie within the range 700-1200°C, and, as a consequence hereof, the heat loss will be relatively large. By recir¬culating the exhaust gas in the way mentioned above afrer -- separation of the from, the separating duct entrained particles and by adding only new exhaust gas to the extent necessary, a substantial reduction in the heat loss car., however, be achieved.
If the separating gas is taken from. the exhaust gas cutlet duct of the preheater it may either be taken immediately after the preheater or after cleaning the exhaust gas in a subsequent filter. The temperature of t.his exnaust gas v;ill cally range between 2C^ anc izZ Z and, therefore :* will be advantageous tc use it for the separation, partly because it has an appropriately high temparature to prerty substantial cooling of the material in the separating duct, and partly because its heat content anyhow will be lost.
The air which is used for cooling a shaft preheater is exhausted at several locations, and, consequently, from a viewpoint of economy/design it v.'ill be less interesting to use this air.
Therefore, it is preferred that the plant according to the invention comprises means, such as dampers, for introducing atmospheric air into the separating duct and/or means, such as pipelines and dampers, for supplying kiln exhaust gas from either the kiln or from the exhaust gas discharge duct of the preheater into the separating duct.

The fine material fraction which entrained in the separa¬ting gas is discharged from the separating duct must be separated from the gas before the latter is either vented to the atmosphere or returned to the separating duct. Accordingly, the plant should incorporate separating means for separating the material from the discharged gas/-material suspension.
The separating means may consist of a separation cyclone
and/or a dedusting filter. As a dedusting filter a bag
filter may be used for separating the fine particles from,
the gas. However, the temperature of the gas/material
suspension will typically be so high, in range between 400
and 600°C, that cold air must be added before the bag
filter, hence reguiring a bigger filter. An electrostatic
precipitator which is normally incorporated in plants of
the mentioned kind for cleaning of the exhaust gas, may
also be used as a dedusting filter. The amount of fine
material being removed from the process by the plant
according to the invention may, however, be relatively
substantial, and, therefore, there may be a risk of the
dedusting filter being overloaded. Further, it is not:
necessarily advantageous to mix the dust'separated from the
exhaust gas v;ith the fine material extracted from rhe
separating gas. It is, therefore, generally preferred that
the gas/material suspension from the separating duct is
initially led to a separation cyclone in which the majority
of the fine material is being separated. The separating ga.s
with the remaining amount of fine material may subseguently
be vented either to the dedusting filter or recirculated
direct to the separating duct. If the separating gas is
vented to the dedusting filter where it will be mixed with
the exhaust gas coming from the preheater, a certain amount
of this mixed gas may be circulated to the separating duct.
Therefore, the plant may incorporate means,-' such as
pipelines, for recirculating the gas from the separation
cyclone and/or the dedusting filter back to the separating duct.

Accordingly, the present invention provides a plant for heat treatment of lumpy material such as limestone, other carbonate minerals, cement raw materials or the like, which plant comprises a preheating zone, more particularly a shaft preheater, with at least one material inlet at least one material outlet, at least one inlet for preheating gas, and at least one outlet for used preheating gas, the material is preheated in the preheating zone by means of hot preheating gas from which it is subsequently separated, a burning zone, e.g. in the form of a rotary kiln, with material inlet and outlet, tor burning the preheated material, connecting means which connect the material outlet of the preheating zone to the material inlet of the burning zone, and a separating device fitted in connection with the connecting means for separating the finest particles from the preheated material, characterized in that the separating device is provided as a part of the connecting means and consisting of a duct, with gas introducing means being provided at the lower end of the duct and with means for discharge of gas/material suspension being provided at the upper end of the duct, and in that the plant comprises means for generating a gas stream through the duct from below and upwards.

The invention will now be described in further details with
accompanying reference to the drawings, being diagrammatical, and where
Fig. 1 shows an example of a plant according to the invention, and
Fig. 2 shows an alternative the plant depicted in Fig. 1 .
The plant shown in Fig. 1 comprises a preheater 1 and a kiln 3. The preheater which is preferably a shaft preheater has a material inlet 5, a material outlet 7, an inlet 9 for preheating gas and an outlet 11 for used preheating gas. The kiln 3, v.'hich may be a rotary kiln, comprises a material inlet 13 and a material outlet 15. Furthermore, the kiln comprises a burner 17. The gas which is used to preheat the material which is to be treated is normally exhaust gas which from the kiln 3 is led to the preheater via one or several ducts 19.
The preheated material is led from the preheater 1 to the
kiln 3 via a feed duct 20. According to the invention ?.
part of this feed duct 20 is configured as a preferably
vertical gas separating duct 21 through v;hich a separating
/Upwards . gas flows/ from below - The separating gas is
introduced via an opening 23 fitted at the bottom of the
duct 20.-and then flows up through the duct 20 at a specifi-
I ed velocity, whereby it captures and entrains the finest
particls in the counter-flowing kiln feed material. The
gas/material suspension thereby formed is discharged via an
opening 25 at the top of the duct 20.
r
In order to attain a satisfactory dispersion and sorting of the material, a dispersion device 27 is fitted in the separating duct 20 in the form of a spreader plate arrange-

ment to ensure that the material is effectively dispersed in the gas stream.
The shown plant further comprises a separation cyclone 31, a dedusting filter 33, and fans 35, 36 and 37 for drawing the various gas streams through and/or around in the plant.
In Fig. 1 there are several alternatives both with respect to the routing of the discharged gas/material and as regards the extraction points of the gas being used as a separating gas. In actual practice, the plant must not necessarily incorporate all the shown alternatives.
The gas/material suspension may be directed from the separating duct 21 via e duct 41 to the separation cyclone 31 in which most of the material is separated and diverted via an opening 32. From the separation cyclone the gas may either be recirculated via a duct 43 and the fan 37 to the

separating duct or directed via a duct 45 to the exhaust gas outlet duct 49 of the preheater 1, in which, mixed with the exhaust gas from the preheater 1 and by means of the fan 35, the gas is vented to the dedusting filter 33. The cleaned gas discharged from the dedusting filter may either be vented to the atmosphere or via a duct 51 and. or 52 circulated to the separating duct 31. Alternatively, the gas/material suspension may via a duct 47 and the duct 49 be vented direct to the dedusting filter.
The separating gas may be taken from the exhaust gas outlet duct 49 of the preheater 1, and be directed via a duct 57 and the fan 36 to the separating duct 21. The separating gas may also be taken from the kiln 3 and directed either via a duct 55 or via the material feed duct to the separa¬ting duct. Further, the separating gas may be taken from one or several of the ducts 19 and directed to the separa¬ting duct via a duct 58. A further possibility is to introduce the gas as atmospheric air which can be done via

damper 53. During operation of the plant, it may be desirable to use as separating gas a gas which is recir¬culated from the dedusting filter 33 via the duct 51 and/or from the separation cyclone 31 via the duct 43 and to use additional separating gas from the aforementioned possibi¬lities only on a supplemental basis or for regulation of the operating conditions, including the temperature of the separating gas.
For regulation of the gas streams in the various ducts, these ducts are provided with dampers 61.
In some plants which handle material types where the finest material tends to stick to the larger lumps of material and thus being less easily suspended and entrained in the separating gas in the separating duct, it may be advantage¬ous, as shown in Fig. 2, to install an air-permeable bottorr, . plate 71 in the separating duct, so that the operating principle of the latter corresponds to that of a fluid bed. As a result, the retention time of the material in tne separating duct will be increased, causing a greater ion of the finest material to be entrained by the separating gas. In this embodiment, it will be impossible for the coarse material to fall through, and, consequently, it must be extracted from the side of the separating duct via means 73 provided for this purpose, subsequently being :ted to the material inlet of the kiln.


WE CLAIM:
1. A plant for heat treatment of lumpy material such as limestone, other carbonate minerals, cement raw materials or the like, which plant comprises a preheating zone (1), more particularly a shaft preheater, with at least one material inlet (5), at least one material outlet (7), at least one inlet (9) for preheating gas, and at least one outlet (11) for used preheating gas, the material is preheated in the preheating zone (I ) by means of hot preheating gas from which it is subsequently separated, a burning zone (3), e.g. in the form of a rotary kiln, with material inlet (13) and outlet (15), for burning the preheated material, connecting means (20) which connect the material outlet (7) of the preheating zone to the material inlet (13) of the burning zone, and a separating device (21) fitted in connection with the coimecting means for separating the finest particles from the preheated material, characterized in that the separating device (21) is provided as a part of the connecting means (20) and consisting of a duct (21), with gas introducing means (23) being provided at the lower end of the duct and with means (25) for discharge of gas/material suspension being provided at the upper end of the duct, and in that the plant comprises means (35, 36, 37) for generating a gas stream through the duct (21) from below and upwards.
2. The plant according to claim 1, wherein the separating duct (21) is vertical.
3. The plant according to claim 1 or 2, wherein a dispersing device (27) is provided in the separating duct (21), e.g. in the form of a spreader plate arrangement.
4. The plant according to claim 1 or 2, wherein the means (35, 36, 37) for generating a gas stream through the duct (21) consist of a fan which is connected to the gas introducing means (23) and/or the gas/material discharge means (25) of the separating duct.

The plant according to claim 1 or 2, wherein the plant comprises means (35,
36,37, 61) for regulating the gas velocity through the separating duct (21).
The plant according to claim 5, wherein the means for regulating the gas
velocity consist of a fan (35,36,37) and/or dampers (61).
The plant according to claim 1 or 2, wherein it comprises means (53), such as
dampers is provided, for introducing atmospheric air into the duct.
The plant according to claim 1 or 2, wherein it comprises means (55, 57, 58,
61), such as pipelines and dampers, for introducing kiln exhaust gas either from
the smoke chamber of the kiln (3), from an exhaust gas duct (19) which
connects the smoke chamber of the kiln and the preheater or from the exhaust
gas duct (49) into the separating duct (21).
The plant according to claim 1 or 2, wherein it comprises separating means (31,
33) for separating the material from the discharged gas/material suspension.
The plant according to claim 9, wherein the separating means consist of a
separation cyclone (31) and/or a dedusting filter (33) such as for example an
electrostatic precipitator or a bag filter.
The plant according to claims 9-10, wherein it incorporates means (43, 51, 52),
such as pipelines, for recirculating the gas back to the separating duct (21).
The plant according to claim 1 or 2, wherein an air-permeable bottom plate
(71) is fitted in the separating duct (21) so that the operating principle of the
separating duct (21) corresponds to that of a fluid bed, and in that means (73)
are provided in the side wall of the separating duct for extraction of the coarsest
material deposited on the bottom plate.
A plant for heat treatment of lumpy material substantially as herein described,
with reference to the accompanying drawings.
Dated this 16* day of June 1995.
(MVG MENON) OF DePENNING & DePENNING AGENT FOR THE APPLICANTS
Dated this 16* day of June 1995.
(MVG MENON) OF DePENNING & DePENNING AGENT FOR THE APPLICANTS

Documents:

728-mas-95 abstract.pdf

728-mas-95 claims.pdf

728-mas-95 correspondences-others.pdf

728-mas-95 correspondences-po.pdf

728-mas-95 description (complete).pdf

728-mas-95 drawings.pdf

728-mas-95 form-1.pdf

728-mas-95 form-4.pdf

728-mas-95 others document.pdf

728-mas-95 others.pdf


Patent Number 190110
Indian Patent Application Number 728/MAS/1995
PG Journal Number 30/2009
Publication Date 24-Jul-2009
Grant Date 08-Mar-2004
Date of Filing 16-Jun-1995
Name of Patentee M/S. MOBIL OIL CORPORATION
Applicant Address 3225 GALLOWS ROAD FAIRFAX VIRGINIA 22037
Inventors:
# Inventor's Name Inventor's Address
1 GREGORY PATRICK MULDOWNEY 39 MILL RACE PLACE, GLEN MILLS, PA 193 1334
2 RONALD ALVIN WEISS 39 MILL RACE PLACE, GLEN MILLS, PA 193 1334
3 JULIAN ALEX WOLFENBARGER 39 MILL RACE PLACE, GLEN MILLS, PA 193 1334
PCT International Classification Number B01J 8/00
PCT International Application Number N/A
PCT International Filing date
PCT Conventions:
# PCT Application Number Date of Convention Priority Country
1 NA