Title of Invention

"A PROCESS FOR PRESERVATION OF FLAVOURED SUGARCANE JUICE"

Abstract The present invention provides a method wherein flavoured sugarcane juice containing 18-20% soluble solids and can be preserved after suitable dilution in aseptic unit packs.
Full Text FLAVOURED SUGARCANE JUICE IN ASEPTIC UNIT PACKS
Technical Field
This invention relates to a process for preservation of sugarcane juice. The process, in
particular, relates to the method of preservation of flavoured sugarcane juice in
aseptic unit packs. By following the process of the present invention, sugarcane juice
containing 18-20% soluble solids and can be preserved after suitable dilution. The
product is derived purely from natural plant material and imparts health benefits to the
consumers. The juice with its delicate aroma is a refreshing beverage, which the
consumers prefer to synthetically flavoured beverages.
Background Art
India is the original home of sugarcane and second largest producer next to Brazil.
Presently, India produces about 280 million tonnes of sugarcane in an area of 4
million hectares. About 10 -12% is available for the manufacture of sugarcane juice.
It is a well known fact that sugarcanes are crushed to obtain juice and it is a common
practice in India to dispense this juice fresh either as such or with the addition of lime
juice and/or fresh ginger extract in glasses by the vendors/hawkers to the consumers.
The major problem encountered in this operation is the lack of hygiene resulting in
contamination of the juice with the heavy load of microorganisms, which arise due to
improper cleaning of the sugarcanes and handling of the finished product. Raw
sugarcane juice is a carbohydrate rich, low acid food and is therefore susceptible to
the growth of yeasts, of spoilage bacteria and also of pathogenic bacteria. Pathogens
such as Salmonella, S.aureus, C.perfringens are able to grow and proliferate at a pH
of more than 4.6. Contamination of raw juice by these bacteria can occur by the food
handlers, by the equipment used or by the environment in which it is prepared. Such
freshly crushed juice cannot be preserved even for a few hours since it is known to
ferment very quickly.
Attempts have been made by many to develop a process for preserving the sugarcane
juice. Yet there is no knowledge / information regarding its manufacture and sale in
any form of packaging material commercially.
Reference may be made to CFTRI process (Shankaranarayana, M.L., Abraham, K.O
andRaghavan, B, CFTRI Annual Report, 1986-87, p 70) wherein the juice was
subjected to pasteurization at 70°C for 10 min. The drawback with the product was
browning and formation of off-flavor not acceptable to consumers.
Reference may be made to Mann and Singh [Mann, R.S and Singh, S. Indian
Farming, 37; 15, 1988] wherein the diluted sugarcane juice containing citric acid and
salt was pasteurized in order to overcome deleterious effects on the consumers. The
drawback of the process was the absence of class II preservatives and low
pasteurization temperature, which resulted in quicker spoilage even at refrigerated
temperature.
Reference may be made to Bhupinder et al., [Bhupinder, K., Sehgal, V.K., Sekhon,
K.S. and Sharrna, K., Proc IIIFCON, CFTRI, 1988, p. 105} wherein a ready to serve
bottled sugarcane juice beverage was developed. The drawback of this process was
the absence of citric acid in the beverage and also pasteurization for 10 minutes at
80°C which is insufficient to preserve the beverage. Also, this is in-pack sterilization
and not aseptic unit packs and hence is different from the present invention.
Reference may also be made to Bhupinder et al. [Bhupinder, K., Sharma, K.P and
Harinder, K., Int. J Trop Agric., 9, p. 128, 1991] wherein the above process was
slightly modified by addition of potassium metabisulphite (sulphur dioxide 70 ppm)
and bottling followed by sterilization for 30 minutes. The drawback with this process
was extended pasteurization time, which will result in flavour deterioration.
Reference may be made to another process involving direct heating of the juice to
85°C for one minute [Sivasubramanian, G. and Pai, J.S., Ind. Food Packer, XLVIII
(2), 51, 1994]. But the resultant product had an off-flavour on storage.
Among the 19 patents related to sugarcane juice that are available, only one relates to
a method for preparing a sugarcane juice based fruit juice and a drink containing said
juice [L.Fahrasmane and M.Catherine WO2000FR0000765, October 5, 2000/March
27 2000]. The above invention consists of atleast one tangential filtration stage for a
dry pressed raw sugarcane extract. One more Indian patent has also been filed under
the title "Preservation process for improved shelf life of sugarcane juice (pure)
[K.P.Sharma, 184435, August 26 2000].
It is evident from the above cited literature that there is no patent or published
information regarding flavoured sugarcane juice in aseptic unit packs.
Objects of the Present Invention
The main object of the present invention is to provide a process for preservation of
flavored sugarcane juice in aseptic unit packs.
Another object of present invention is to provide a compatible flavor blend
comprising of ginger and lime / lemon that can be incorporated into sugarcane juice to
provide a better aroma and mouth feel.
Summary of the Invention
Accordingly, the present invention relates to a process for preparing flavored
sugarcane juice and storage of the flavored sugarcane juice in aseptic unit packs.
Brief Description of the Accompanying Drawings
In the drawings accompanying the specification,
Figure 1 represents the flow chart of the process for the preservation of sugarcane
juice in aseptic unit packs.
Figure 2 shows the material balance of the constituents obtained for Example 3.
Detailed Description of the Present Invention
The present invention provides a process for preservation of flavored sugarcane juice,
the said process comprising:
a) soaking the canes in water containing 0.1% by wt. potassium metabisulphite
and 0.01% by wt. citric acid for a period of 2-4 hrs,
b) washing the soaked sugarcanes of step (a) and crushing the same to obtain
sugarcane juice having 18-20° Brix, and filtering the sugarcane juice,
c) adjusting the total solid content of the filtered sugarcane juice of step (b) to
10-16° Brix by adding soft beverage water,
d) acidifying the sugarcane juice of step (c) by adding 0.1-0.3% by wt. citric
acid and 0.01-0.03% by wt. sodium citrate,
e) adding to the acidified sugarcane juice of step (d) a flavor blend consisting of
0.05-0.20% by wt. of ginger oleoresin and/or 0.01-0.05% by wt. of essential
oils of lime and lemon to obtain a flavored sugarcane juice,
f) blending the flavored sugarcane juice of step (e) and pasteurizing the same at
90-110°C for 30-180 sec to obtain the flavored sugarcane juice which may be
filled in aseptic unit packs.
In an embodiment of the present invention, wherein in step (b), the sugarcanes are
washed with plain water before crushing.
In another embodiment of the present invention, wherein the sugarcanes are crushed
using mechanical devices.
In yet another embodiment of the present invention, wherein in step (b), the sugarcane
juice is filtered using muslin cloth.
In still another embodiment of the present invention, wherein in step (c) the sugarcane
juice is diluted with beverage water to adjust the sweetness at 15%.
In another embodiment of the present invention, wherein in step (d), the sugarcane
juice is acidified by adding 0.2% by wt. citric acid and 0.02% by wt. sodium citrate.
The process for the preservation of sugarcane juice in aseptic unit packs is illustrated
in Figure 1. The novelty of the process lies in the combined manner in which critical
steps such as pre-treatment of the sugarcanes, homogenization of the juice with a
flavor blend consisting of ginger and lime-lemon flavors in such a manner as to
dispense the flavor in the bulk of the juice and pasteurization at specific temperature
for a particular duration are carried out in order to preserve the sugarcane juice. It has
been found that by following the process as described above, the Inventors have been
successful in preserving the natural taste of sugarcane juice without browning and offflavoring
the sugarcane juice.
The applicability of the process is further illustrated in the following examples which
are given by way for illustrating the present invention in a much better manner and
hence, should not be construed to limit the scope of the present invention in any
manner.
Example 1
Sugarcanes (1.2 tonnes) were procured, roots and stems trimmed to obtain 1 tonne of
cleaned canes. These were soaked in KMS solution for 2 hours. Then the canes were
thoroughly washed and juice extracted using the twin roller crusher with SS rollers.
500 L of juice (20 °Brix) was obtained and collected in a chiller tank with recirculation
facility, maintained at 4°C. The brix was brought down to 15.4 by adding
soft water (150 L). The product was thawed, pH adjusted to 3.70 by adding citric acid
(0.2%) and sodium citrate (0.02%). The total quantity of juice was 650 L. After pH
and brix adjustment, the juice was pumped to homogeniser at 140 bar and
subsequently to sterilizer to pasteurize at 95°C for 60 s. Pasteurized juice was stored
in an aseptic tank with steam locks. Meanwhile, the filling section of the processor
was sterilized with superheated water. Subsequently, the juice was filled into 250 ml
aseptic unit packs.
Example 2
Sugarcanes (1.4 tonnes) were thoroughly cleaned to remove the waxy layer by
scraping the rind. The final weight of the cleaned canes were 1050 kg and were
soaked in KMS solution for 4 h. The canes were washed with running water and
crushed to obtain 510 liters of juice (20°Brix). The juice was diluted to 15.2°Brix by
adding soft water (160L). Citric acid (0.2%), sodium citrate (0.02%) and flavour
blend (500 ml) consisting of ginger oleoresin (70 g) duly emulsified in propylene
glycol were added. The juice was pumped to homogeniser at 140 bars through deaerator
and subsequently to sterilizer and pasteurized at 105°C for 60 s. Subsequently,
the juice was filled into 250 ml aseptic unit packs.
Example 3
1.2 tonnes of canes were procured, roots and stem were trimmed. The sugarcanes
were thoroughly cleaned to remove the waxy layer by scraping the rind. The cleaned
canes were soaked in KMS solution for 4 h. The canes were washed with running
water, crushed to obtain about 480 liters of juice (17 °Brix) followed by dilution with
soft water (55 L) to adjust the brix to 15.2°. Citric acid and sodium citrate at the levels
of 0.2 and 0.02% respectively and a flavour blend (500 ml) consisting of ginger
oleoresin (70 g) and terpeneless lime and lemon oil (7.5 ml each) duly emulsified in
propylene glycol was added to the juice and pumped to the homogeniser at 140 bars
through de-aerator and subsequently to sterilizer for pasteurization at 95°C for 60 s.
Subsequently, the juice was filled into 250 ml aseptic unit packs. The material balance
for example 3 is shown in figure 2.



Claims
1. A process for preservation of flavored sugarcane juice, the said process
comprising:
a) soaking the canes in water containing 0.1% by wt. potassium
metabisulphite and 0.01% by wt. citric acid for a period of 2-4 hrs,
b) washing the soaked sugarcanes of step (a) and crushing the same to
obtain sugarcane juice having 18-20° Brix, and filtering the sugarcane
juice,
c) adjusting the total solid content of the filtered sugarcane juice of step
(b) to 10-16° Brix by adding soft beverage water,
d) acidifying the sugarcane juice of step (c) by adding 0.1-0.3% by wt.
citric acid and 0.01-0.03% by wt. sodium citrate,
e) adding to the acidified sugarcane juice of step (d) a flavor blend
consisting of 0.05-0.20% by wt. of ginger oleoresin and/or 0.01-0.05%
by wt. of essential oils of lime and lemon to obtain a flavored
sugarcane juice,
f) blending the flavored sugarcane juice of step (e) and pasteurizing the
same at 90-110°C for 30-180 sec to obtain the flavored sugarcane juice
which may be filled in aseptic unit packs.
2. A process as claimed in claim 1, wherein in step (b), the sugarcanes are
washed with plain water before crushing.
3. A process as claimed in claim 1, wherein the sugarcanes are crushed using
mechanical devices.
4. A process as claimed in claim 1, wherein in step (b), the sugarcane juice is
filtered using muslin cloth.
5. A process as claimed in claim 1, wherein in step (c) the sugarcane juice is
diluted with beverage water to adjust the sweetness at 15%.
6. A process as claimed in claim 1, wherein in step (d), the sugarcane juice is
acidified by adding 0.2% by wt. citric acid and 0.02% by wt. sodium citrate.
7. A process for preservation of flavored sugarcane juice substantially as herein
describe with reference to examples accompanying this specification.

Documents:

407-DEL-2003-Abstract-(17-12-2007).pdf

407-del-2003-abstract.pdf

407-DEL-2003-Claims-(17-12-2007).pdf

407-del-2003-claims.pdf

407-DEL-2003-Correspondence-Others-(03-03-2008).pdf

407-DEL-2003-Correspondence-Others-(09-01-2008).pdf

407-DEL-2003-Correspondence-Others-(17-12-2007).pdf

407-del-2003-correspondence-others.pdf

407-del-2003-correspondence-po.pdf

407-DEL-2003-Description (Complete)-(17-12-2007).pdf

407-del-2003-description (complete).pdf

407-del-2003-drawings.pdf

407-DEL-2003-Form-1-(03-03-2008).pdf

407-DEL-2003-Form-1-(17-12-2007).pdf

407-del-2003-form-1.pdf

407-del-2003-form-18.pdf

407-DEL-2003-Form-2-(17-12-2007).pdf

407-del-2003-form-2.pdf

407-DEL-2003-Form-3-(17-12-2007).pdf

407-del-2003-form-3.pdf

407-DEL-2003-Petition-137-(09-01-2008).pdf


Patent Number 216709
Indian Patent Application Number 407/DEL/2003
PG Journal Number 13/2008
Publication Date 28-Mar-2008
Grant Date 18-Mar-2008
Date of Filing 26-Mar-2003
Name of Patentee COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH.
Applicant Address RAFI MARG, NEW DELHI-110 001,INDIA.
Inventors:
# Inventor's Name Inventor's Address
1 BASHYAM RAGHAVAN CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
2 MYSORE NAGARAJARAO RAMESH CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
3 KULATHOORAN RAMALAKSHMI CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
4 NANJUNDAIAH KRISHNAMURTHY CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
5 PRAKASH MURALIDHAR BADGUJAR CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
6 VISHWESHWARAIAH PRAKASH CENTRAL TECHNOLOGICAL RESEARCH INSTITUTE,MYSORE INDIA
PCT International Classification Number A23L 3/00
PCT International Application Number N/A
PCT International Filing date
PCT Conventions:
# PCT Application Number Date of Convention Priority Country
1 NA