Title of Invention

A LIQUID DISTRIBUTOR FOR COLUMNS

Abstract A liquid distributor (1) for columns (6) having a main passage (2), a plurality of secondary passages (3) and an outflow system (5) of the main passage with which the liquid (4) to be distributed can be fed into the secondary passages in accordance with a pre-set ratio, wherein the outflow system (5) includes apertures (20) in the side walls of the main passage and-associated with the secondary passages-guide elements (50) for the liquid (41) exiting through the apertures, with the guide elements being designed with respect to a liquid guidance such that the liquid (42) can be led into the associated secondary passage, characterized in that each guide element (50) has a cross-section which brings about the liquid guidance and which narrows in the direction of flow; and in that the liquid guidance substantially only influences the horizontal speed component and leaves the speed component in the direction of the secondary passage (3) largely unaffected.
Full Text FORM 2
THE PATENTS ACT 1970
[39 OF 1970]
COMPLETE SPECIFICATION
[See Section 10]
"A LIQUID DISTRIBUTOR FOR COLUMNS"
SULZER CHEMTECH AG, of Hegifeldstrasse 10, CH-8404 Winterthur, Switzerland,
The following specification particularly describes the nature of the
invention and the manner in which it is to be performed:-


The present invention relates to a liquid distributor columns.
The invention relates to a liquid distributor for columns in accordance with the preamble of claim 1 and to a column having such a liquid distributor, with the column being provided for a material exchange between a gas flow and a liquid flow flowing on a packing. The invention aloo relates te-a method of operation and manufacti-iring of-a liquid distributor.
It is necessary for a good efficiency of the column that no' mal-distribution of the liquid occurs, that is that the liquid trickles in a'homogeneously distributed manner over the surfaces inside the packing. For a mal¬distribution not to take place, the liquid must be poured onto the packing in an even and sufficiently fine distribution. This is possible by means of a suitably designed liquid distributor by which the liquid is "distributed onto the packing via a passage system and using outflow systems.
In a known liquid distributor, which has been given the name "element distributor", the passage system consists of a main passage and a plurality of secondary passages which are arranged beneath the main passage. The liquid to be distributed is fed into the secondary passages in a pre-set ratio by an outflow system of the main passage. This ratio is, as a rule, equal to the ratio between the part areas of the packing surface which are associated with the secondary passages and to which liquid is to be distributed in proportion to the area of the part area. The liquid leaves the distributor through an outflow system of the secondary passages. The outflow system of the secondary passages is present, for

example, in the form of a plurality of side openings with drainage pipes or impact plates, or of a plurality of base openings. The outflow system of the main passage of a distributor, which is to be improved, normally consists of hood-like chambers, open to the bottom, which are arranged in the bottom of the main passage above rectangular openings corresponding to the second passages, with the lower edges of the chambers being sealingly connected, as a rule those of the openings. Apertures in the side wails of these chambers allow the liquid exiting the main passage to flow into the associated secondaiy passages. During this inflow, choppy flow fields result which become disturbingly noticeable in the form of a fluctuating outflow in the outflow system of the secondaiy passages. The disadvantage exists with respect to the main passage that the hood-like chambers restrict the cross-section of the passage which is available for the flow of the liquid to be distributed and that the construction is relatively expensive due to welding work.
It is the object of the invention to provide a favourably priced liquid distributor of the "element distributor" type in which the liquid flows through the main passage unhindered by an outflow system and is led into the secondary passages such that it enters into the outflow systems of the secondary passages as a calmed flow. This object is satisfied by the liquid distributor which has a main passage, a plurality of secondary passages and an outflow system of the main passage. The liquid to be distributed can be fed into the secondary passages in accordance with a pre-set ratio by this outflow system. The outflow system comprises apertures in the side walls of the main passage and — associated with the

^

secondary passages-guide elements for the liquid exiting through the apertures. The guide elements are designed with respect to a liquid guidance such that the liquid can be led into the respective associated secondary passage.
The further advantageous embodiments of the liquid distributor of the invention have been described in the subsequent pages of the specification. The invention also describes the application of the liquid distributor in a column.
The invention is explained below with reference to the drawings. There are shown:
■ Fig., 1 in a simplified illustration, a known liquid distributor, having a
main passage and secondary passages;
Fig. 2 sectionally illustrated, a liquid distributor of the invention;
' Fig. 3 . a longitudinal section through the upper part of a column;
Figs. 4, 5 details of three embodiments of the liquid distributor of the invention;
Fig. 6 a plan vievr of a liquid distributor which belongs to the'type
illustrated in Fig. 5; and
Fig. 7 a detail of a snap connection between a guide element and a
secondar)'" passage.

The liquid distributor 1 illustrated in a simplified manner in Fig. 1 is a known "element distributor"; it comprises a main passage 2 and secondary passages 3 which are open to the top. Constructive elements
outflow system 30 of the secondary passages 3, through which a liquid 4 is poured onto a packing 7 (see Fig. 3) in a uniform distribution and which one can imagine as consisting of base openings in the distributor 1 shown, is likewise not illustrated.
A wall part, which is broken open, reveals the above-described outflow system of the main passage 2. This consists of hood-like charribers 21 which are arranged at the floor of the main passage 2 above openings. Lower edges of the chambers are sealingly connected to the edges of the openings. Apertures 22 allow the liquid 4 exiting the main passage 2 to flow into the secondary passages 3 associated with the chambers 21.
With the liquid distributor 1 illustrated sectionally in Fig. 2, an outflow system 5 of the main passage 2 can be recognised with which the liquid to be distributed can be fed into the secondary passages in accordance with a pre-set ratio. It is a liquid distributor 1 in accordance with the invention, in which the outflow system 5 comprises apertures 20 in the side walls of the main passage 2 and - associated with the secondary passages 3 -guide elements 50 for the liquid 41 (Fig. 3) exiting through the apertures 20. In contrast to the outflow system shown in Fig. 1, this outflow system 5 no longer forms an obstacle for the liquid 4 flowing in the main passage 2.

The apertures 20 correspond in number and size to the pre-set ratio in accordance with which the liquid 4 is to be distributed into the secondary passages.
The cross-section narrows in the flow direction in each guide element 50 and with this shape brings about the liquid guidance with which the liquid 4 enters into the associated secondary passage 3 in the form of a jet 42 without loss. Essentially only the horizontal speed component of the liquid jet 41 exiting the main passage 2 is influenced by the liquid guidance in the guide element 50. The speed component in the direction of the secondary passage 3 remains largely unaffected. The liquid jet 41 enters the secondary passage 3 with a large horizontal speed component and a small vertical speed component such that a calmed, even flow is formed there. A distribution thus results for the liquid 44 flowing out of the outflow system 30 of the secondary passages 3 which is subject only to slight fluctuations: the liquid distribution is of low fluctuation.
In the distributor 1 of the invention, the apertures 20 can be arranged distributed over the whole longitudinal extent of the main passage. This allows a positioning of the apertures 20 at relatively large intervals so that a mutual influencing of adjacent apertures 20 is smaller than if the apertures 20 were arranged very close to one another.
The longitudinal section through the upper part of a column 6 (with the column wall 60) illustrated in Fig. 3 shows a main passage 2 in cross-section, a secondary passage 3 in longitudinal section and the upper part of an ordered package 7, which is composed, for example, of corrugated material surfaces - forming a cross-passage structure. The liquid 4 to be

treated is fed into the main passage 2 (arrow 40) via a pipe 10 and distributed from there via the guide elements 50 into the secondary passages 3. The liquid 4 is there supplied in a largely uniform manner to the outflow system 30 (not shov/n) via circulating flov,'S 43 v/hich are driven by the liquid jets 42.
In Figures 4 and 5, details of three embodiments of the liquid distributor of the invention are illustrated which differ by differently formied guide elements 50, 50' a.nd 50". As a_ rule, a uniform type of guide organ - in contrast to Fig. 4 - is used. To better illustrate the construction, the front parts 50a of the guide elements 50, 50', 50" are shown in cut-away manner in each case as well as the corresponding parts of the secondary passages 3. The side edges of the cut-away parts 50a and the front edge 500 are indicated in chain-dotted lines. The upper side edges 31 of the secondary passages 3 are likewise indicated in chain-dotted lines.
As a rule, one guide element 50 or 50' each is associated with each secondary passage 3 in a symmetrical manner at the two longitudinal sides of the main passage 2. It is, however, also possible, for example, for only one guide element 50" each - see Fig. 6 - to be associated with the secondary passages 3 in an offset arrangement of the guide elements 50".
The first guide element 50 in Fig. 4 corresponds to those shown in Fig. 2. This guide element 50 and the second guide element 50' are each manufactured from a suitably shaped piece of sheet metal by forming. They are formed in a mirror-symmetrical manner with respect to a vertical plane directed in the longitudinal extent of the secondary passage 3.

The guide element 50 is closed to the top: it consists of a slanting roof surface 51, two vertical flanks 52, two triangular part areas 52 and two flanks 54 which are inserted under a pre-stressing between the side areas
passage through the apertures 20, is first guided downwardly from the roof surface 51 at a flat angle and led through the wall 52, 53 of the guide element 50 to the front edge 500, where it enters into the secondary-passage 3 - distributed over its width.
The guide element 50' is open to the top and has the following part areas: vertical side surfaces 52', slanting triangular surfaces 53', vertical wall pieces 54', which project into the secondary passage 3, and a horizontal connection surface 55'. Parabolic liquid jets 41, which exit the apertures 20, impact directly, or guided by the wall 52', 53', onto the connection surface 55', on which the liquid 4 continues to flow into the inner space of the secondary passage 3.
Fig. 5 shows an asymmetrically formed guide element 50" which extends over two adjacent secondary passages 3. It has the following part areas: an upper side 51", side flanks 52" and 520" and a triangular surface 53". This guide element 50" is suitable for a distributor 1 such as is shown as a plan view in Fig. 6. Symmetrical guide elements 50 - two each per, secondary passage - can also be provided in a middle region and asymmetrical guide elements 50" in the outer regions.
The outflow system 5 of the secondary passages 3 allows a connection technique to be used in the manufacture of the distributor 1 of the invention in which the guide elements 50 of the outflow system 5 form

only form-locked connections to the main passage 2 and to the secondary passages 3. The guide elements 50, 50' and 50" are set onto their associated secondary passages 3, with sealing connections, in particular weld seamxS, no longer being necessary. This allows a low-cost manufacture. It is also of advantage for the guide elements 50 to be installed at the location of use. They can likewise be dismantled there, which allows a good accessibility for a cleaning of the distributor 1.
The guide elements 50 set onto the secondary passages 3 a.re prefera.bly fixed to the side walls 35 of the secondary passage 3 in each case by means of a releasable snap or plug connection. The one half of such a snap connection is shown in Fig. 7. A tong ue 540, which can be deflected out of the plane of the flank 54 in a resiliently elastic manner, is provided in the lower flank 54 of the guide element 50 illustrated in Fig. 4. An aperture 541 is included in this tongue 540, said aperture 541 having a straight lower edge 542. When the guide element 50 is pushed onto the secondaiy passage 3 (arrow 530), the tongue 540 slides on the side wall 35 of the secondaiy passage 3, with the two end points of the edge 542 moving on the lines 350 shown in chain-dotted manner. An elevation 351 of the side wall 35 produced by embossing, which has an edge 352 projecting into the inner space of the secondaiy passage 3, latches into the aperture 541 of the tongue 540. The two edges 542 and 352 are formed and arranged such that they come to lie flush next to one another in the lowest possible position of the tongue 540 and thus make a snap connection. A corresponding snap connection is also provided for the parallel side wall of the secondary passage 5 not shown in fig. 7. After a latching of the elevation 351 in the aperture 541, the elastic tongue 540 can be raised somewhat in order to thus release the snap connection.

WE CLAIM:
1. A liquid distributor (1) for columns (6) having a main passage (2), a
plurality of secondary passages (3) and an outflow system (5) of the main
passage with which the liquid (4) to be distributed can be fed into the
secondary passages in accordance with a pre-set ratio, wherein the outflow
system (5) includes apertures (20) in the side walls of the main passage and-
associated with the secondaiy passages-guide elements (50) for the liquid
(41) exiting through the apertures, with the guide elements being designed
with respect to a liquid guidance such that the liquid (42) can be led into the
associated secondary passage, characterized in that each guide element (50)
has a cross-section which brings about the liquid guidance and which
narrows in the direction of flow; and in that the liquid guidance
substantially only influences the horizontal speed component and leaves the
speed component in the direction of the secondary passage (3) largely
unaffected.
2. A liquid distributor (1) as claimed in claim 1, wherein the guide elements (50) are set onto their associated secondary passages (3) and are preferably fixed at the side walls (35) of the secondary passage by means of a releasable snap connection (352, 542).
3. A liquid distributor (1) as claimed in any of claims 1 to 2, wherein two guide elements (50; 50') are associated with each secondary passage (3) in a symmetrical manner; or in that only one guide element (50") each is associated with the secondary passages in an offset arrangement of the guide elements.
4. A liquid distributor (1) as claimed in any of claims 1 to 3,
wherein the guide elements (50; 50') are formed with mirror symmetry
and/or in an asymmetrical manner with respect to a vertical plane directed
in the longitudinal extent of the secondary passages (3).

5. A liquid distributor (1) as claimed in any of claims 1 to 4,
wherein the guide elements (50, 50', 50") are each manufactured by forming
from a suitably shaped piece of sheet metal.
6. A liquid distributor (1) as claimed in claim 5, wherein the guide elements (50, 50") are closed to the top,
7. A liquid distributor (1) as claimed in claim 5, wherein the guide elements (50') are open to the top.
8. A liquid distributor (1) as claimed in any of claims 1 to 7 wherever
incorporated in a column (6).
9. A liquid distributor (1) for columns substantially as hereinbefore
described with reference to the accompanying drawings.

[P.SEETHA]
OF REMFRY & SAGAR
ATTORNEY FOR THE APPLICANT[S]
Dated this 26 day of March, 2008
isi

Documents:

293-mum-2002-abstract(7-4-2008).doc

293-mum-2002-abstract(7-4-2008).pdf

293-mum-2002-cancelled pages(5-11-2007).pdf

293-mum-2002-claims(granted)-(7-4-2008).doc

293-mum-2002-claims(granted)-(7-4-2008).pdf

293-MUM-2002-CORRESPONDENCE(26-3-2010).pdf

293-mum-2002-correspondence(7-4-2008).pdf

293-mum-2002-correspondence(ipo)-(3-4-2008).pdf

293-mum-2002-drawings(5-11-2007).pdf

293-mum-2002-form 1(26-3-2002).pdf

293-mum-2002-form 1(5-11-2007).pdf

293-mum-2002-form 13(1-4-2008).pdf

293-mum-2002-form 13(5-11-2007).pdf

293-mum-2002-form 18(27-2-2006).pdf

293-mum-2002-form 2(granted)-(7-4-2008).doc

293-mum-2002-form 2(granted)-(7-4-2008).pdf

293-MUM-2002-FORM 26(26-3-2010).pdf

293-mum-2002-form 3(15-7-2002).pdf

293-mum-2002-form 3(26-3-2002).pdf

293-mum-2002-form 3(5-11-2007).pdf

293-mum-2002-form 3(8-3-2006).pdf

293-mum-2002-form 5(26-3-2002).pdf

293-mum-2002-petition under rule 137(5-11-2007).pdf

293-mum-2002-petition under rule 138(5-11-2007).pdf

293-mum-2002-power of authority(29-5-2002).pdf

293-mum-2002-power of authority(5-11-2007).pdf

abstract 1.jpg


Patent Number 221000
Indian Patent Application Number 293/MUM/2002
PG Journal Number 41/2008
Publication Date 10-Oct-2008
Grant Date 11-Jun-2008
Date of Filing 26-Mar-2002
Name of Patentee SULZER CHEMTECH AG
Applicant Address HEGIFELDSTRASSE 10, CH-8404 WINTERTHUR.
Inventors:
# Inventor's Name Inventor's Address
1 EMIL FEHR DORFSTRASSE 47, CH-8415 BERG AM IRCHEL,
2 ADRIAN FAUST LOHSTRASSE 32, CH-8362 BALTERSWIL.
3 MARKUS FISCHER MAYENFISCHSTRASSE 13, D-78462 KONSTANZ.
PCT International Classification Number F16K15/00 B01D3/00
PCT International Application Number N/A
PCT International Filing date
PCT Conventions:
# PCT Application Number Date of Convention Priority Country
1 01810510.6 2001-05-23 EPO