Title of Invention

OPTICAL FIBER HAVING REDUCED POLARIZATION MODE DISPERSION (PMD) AND METHOD FOR PRODUCING THE SAME

Abstract N/A
Full Text STER/P A/036
FORM 2
THE PATENTS ACT, 1970 (39 of 1970)
THE PATENTS RULES, 2003 COMPLETE SPECIFICATION
(See Section 10 and Rule 13)
1. Title of the Invention: -
Optical fiber having reduced polarization mode dispersion [PMD] and method for producing the same.
2. Applicant(s):-
(a) Name: STERLITE OPTICAL TECHNOLOGIES LTD.
(b) Nationality: An Indian Company
(c) Address: E1/E2/E3, MIDC, Waluj, Aurangabad - 431136
Maharashtra, INDIA
3. Preamble to the Description:-Complete Specification:
The following specification particularly describes the Invention and the manner in which it is to be performed.
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Field of the Invention:
The present invention relates to optical fiber having reduced polarization mode dispersion [PMD]. Particularly, it relates to method for producing an optical fiber having reduced PMD. More particularly, it relates to a method for
5 producing optical fiber preform having symmetrically and completely collapsed capillary, which is suitable for producing optical fiber having reduced PMD. Even more particularly, it relates to a method for producing optical fiber preform having symmetrically and completely collapsed capillary, wherein the preform produced has diameter more than about 90 mm or weight more than
10 about 9Kg, and is suitable for producing optical fiber having reduced PMD.
Background of Invention:
Optical fibers are inherently versatile as a transmission medium for all
forms of information, be it voice, video or data. The primary object of
telecommunication industry is to transmit larger amounts of information over
15 longer distances in shorter period of time. In the recent years, certain
improvements have taken place in the light carrying ability of the optical fibers. The light carrying ability of the optical fibers for communication is
primarily determined by attenuation loss and PMD. The optical losses, that is,
attenuation loss in the fiber are caused by many factors including absorption
20 loss, scattering of light, and PMD in fiber are caused by imperfect geometry of
the fiber, stress and structural defects in the fiber. It has been observed that imperfect geometry of the fiber, and stress and structural defects in the fiber are caused due to unsymmetric and incompletely collapsed centerline [capillary] in the optical fiber preform from which the fiber
25 is drawn. The problems of imperfect geometry of the fiber, and stress and structural defects in the fiber is further enhanced if the preform from which the fiber is drawn has unsymmetric and incompletely collapsed centerline [capillary] particularly at middle portion thereof.
Therefore, the need of the time is to have an optical fiber preform which
30 should have symmetrically and completely collapsed centerline [capillary] so
that an optical fiber having reduced PMD can be produced.
The co-pending Indian patent application no. 494/MUM/2004 [IPA494]
defines a process to achieve complete collapsing of the capillary of the preform,
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by simultaneously carrying out sintering and collapsing process steps on the
dehydrated hollow soot porous body. In accordance with this method, preform
having completely collapsed capillary is obtained, but the capillary in the top
portion of the preform is still not completely collapsed.

5 The another co-pending Indian patent application no. 1530/MUM/2005
[IPA1530] defines an improved process to achieve complete collapsing of the capillary of the preform, wherein the simultaneous sintering and collapsing process steps are carried out on the dehydrated hollow soot porous body under specifically controlled heating. In accordance with this method, preform having
10 completely collapsed capillary is obtained, particularly having collapsed
capillary in the top portion of the preform.
It has been observed that both the methods taught in IPA494 and IPA1530 are suitable for achieving complete collapsing of capillary, if the preform prepared has diameter of less than about 90 mm or weight of less than
15 about 9Kg. However, if the preform prepared should have diameter more than about 90 mm or weight more than about 9Kg, then both the methods taught in IPA494 and IPA1530 result in incomplete collapsing of the capillary, particularly in the middle portion.
The methods taught in IPA494 and IPA1530 do not address the problem
20 of unsymmetric collapsing of the capillary and uncollapsed capillary at the middle portion particularly when the preform prepared is of diameter more than about 90 mm or weight more than about 9 Kg.
Need of the Invention:
Therefore, there is a need to have a method for preparing an optical fiber
25 preform having symmetrically and completely collapsed centerline [capillary] so that an optical fiber having reduced PMD can be produced therefrom, and to have an optical fiber having reduced PMD. Further, there is a need to have a method for preparing an optical fiber preform wherein the method is suitable even if the preform should have diameter more than about 90 mm or weight
30 more than about 9 Kg.
Objects of the Invention:
One of the main objects of the present invention is to provide a method for preparing an optical fiber preform having symmetrically and completely
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collapsed centerline [capillary] so that an optical fiber having reduced PMD can be produced therefrom, and to provide an optical fiber having reduced PMD.
The another main object of the present invention is to provide a method for preparing an optical fiber preform wherein the method is suitable even for
5 producing preform of diameter more than about 90 mm or weight more than
about 9 Kg.
Another object of the present invention is to provide a method for preparing an optical fiber preform having symmetrically and completely collapsed capillary, so that an optical fiber having perfect geometry and,
10 reduced stress and structural defects can be produced therefrom, and to
provide an optical fiber having perfect geometry, and reduced stress and
structural defects.
Still another object of the present invention is to provide a method for
preparing an optical fiber preform having symmetrically and completely

15 collapsed capillary, particularly at and around middle portion thereof, so that
an optical fiber having perfect geometry, and reduced stress and structural
defects can be produced therefrom, and to provide an optical fiber having
perfect geometry, and reduced stress and structural defects over its entire
length.

20 Other objects and advantages will be apparent from the following
description when read in conjunction with the accompanying figures.
Brief Description of the Invention:
It is apparent from the foregoing description that the known methods for producing preform are not suitable for producing a preform having
25 symmetrically and completely collapsed capillary, particularly at the middle
portion thereof, and having diameter more than about 90 mm or weight more
than about 9Kg, wherein the preform produced is suitable for producing optical
fiber having reduced PMD.
The present inventors have observed that the collapsing of the capillary

30 in a hollow soot porous body or sintered glass body is carried out while applying
a constant vacuum along entire length of hollow soot porous body or sintered
glass body. It has been observed that the collapsing of capillary under constant
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vacuum results in unsymmetrical and incomplete collapsing of the capillary, particularly at and around its middle portion.
As the mandrel employed in preparation of a preform has tapered diameter for achieving its easy removal from the soot porous body, the prepared
5 hollow soot porous body and the sintered glass body prepared therefrom are
observed to have reducing capillary diameter from one end [referred as top end]
to another end [referred as bottom end] of the soot porous body or sintered
glass body.
The present inventors have observed that the constant vacuum applied
10 in hollow soot porous body or sintered glass body having capillary of reducing
[varying] diameter from one end to another end during the collapsing process
step surprisingly causes unsymmetric and incomplete collapsing of capillary,
particularly at and around its middle portion while producing the optical fiber preform [mother preform]. Such optical fiber preform having unsymmetric and
15 incompletely collapsed capillary has been observed to have imperfect geometry, non-uniform stress and structural defects at its centerline region. It has also been observed that the preform having unsymmetric and incompletely collapsed capillary meaning thereby having imperfect geometry, non-uniform stress and structural defects at its centerline region produces an optical fiber having
20 imperfect geometry, and stress and structural defects.
It has been further observed that during the collapsing step, the hollow soot porous body or sintered glass body gets stretched, particularly at and around its middle portion primarily due to its larger weight and gravitational force. The un-symmetric stretch of the soot porous body or sintered glass body
25 also causes unsymmetric and incomplete collapsing of capillary, particularly at and around its middle portion while producing the optical fiber preform [mother preform], which is observed to have imperfect geometry, non-uniform stress and structural defects at its centerline region. The preform having unsymmetric and incompletely collapsed capillary produces an optical fiber having imperfect
30 geometry, and stress and structural defects.
The present inventors have surprisingly observed that if the collapsing of capillary in a hollow soot porous body or sintered glass body is carried out under a variable vacuum from one end to another end then the capillary
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surprisingly collapses symmetrically and completely over its entire length, including at and around its middle portion meaning thereby it produces the optical fiber preform [mother preform] having perfect geometry, and reduced stress and structural defects at its centerline region, which has been found
5 suitable to produce an optical fiber having imperfect geometry, and stress and structural defects.
Accordingly, in one embodiment, the present invention relates to a method for producing optical fiber preform having symmetrically and completely collapsed capillary which is suitable for producing optical fiber having reduced
10 PMD, comprising collapsing the capillary in the hollow soot porous body or
sintered glass body under variable vacuum to form optical fiber preform having
symmetrically and completely collapsed capillary.
In one embodiment, the present invention also relates to a fiber produced from the preform produced by employing method of the present invention,
15 wherein the fiber produced has reduced PMD.
Other advantages and preferred embodiments of the present invention will be apparent from the following description when read in conjunction with the accompanying figures, which are not intended to limit scope of the present invention.
20 Description of the Accompanying Figures:
Figure 1 illustrates a schematic representation of deposition process over a mandrel to produce a soot porous body.
Figure 2 illustrates a schematic representation of hollow soot porous body having centerline therethrough after removal of mandrel from the soot
25 porous body.
Figure 3 illustrates a schematic cross-sectional view of hollow soot porous body having centerline therethrough after removal of mandrel from the soot porous body.
Figure 4 illustrates a schematic representation of hollow soot porous
30 body inside the sintering furnace after removal of mandrel from the soot porous body.
Figure 5 illustrates a hollow soot porous body having centerline therethrough after removal of mandrel from the soot porous body which is
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subjected to steps of dehydration, and sintering and collapsing to produce a solid glass preform.
Figure 6 illustrates vacuum profile, in accordance with one of the preferred embodiments of the present invention, for simultaneous sintering and
5 collapsing, or collapsing process step to have symmetric and complete collapsing of the capillary to produce a solid glass preform.
Figure 7 illustrates vacuum profile, in accordance with another preferred embodiment of the present invention, for simultaneous sintering and collapsing, or collapsing process step to have symmetric and complete
10 collapsing of the capillary to produce a solid glass preform.
Figure 8 illustrates vacuum profile, in accordance with still another
preferred embodiment of the present invention, for simultaneous sintering and
collapsing, or collapsing process step to have symmetric and complete
collapsing of the capillary to produce a solid glass preform.
15 Figure 9 illustrates PMD of the fiber produced in accordance with
conventional method.
Figure 10 illustrates PMD of the fiber produced in accordance with one of the preferred embodiments of the present invention.
Figure 11 illustrates PMD distribution of the fiber produced in 20 accordance with conventional method.
Figure 12 illustrates PMD distribution of the fiber produced in accordance with one of the preferred embodiments of the present invention.
Detailed Description and Preferred embodiments of the Invention;
Typically, a preform can be manufactured by a conventional method, for
25 example by ACVD method, which is described herein for reference.
In accordance with a typical ACVD process to manufacture a soot porous body, as illustrated in accompanying Figure 1, the preparation of soot porous body 1 comprises the following steps. The glass-forming precursor compounds are oxidized and hydrolyzed to form porous silica based materials 2. The porous
30 silica based materials 2 are deposited on a mandrel 3, which can be any commercially available mandrel with or without any specific preparation, preferably with specific preparation to remove the contaminants therefrom
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which is provided with a handle rod 4 and fitted on a lathe 5 to form soot porous body 1.
During the step of deposition, the mandrel 3 is rotated in a direction as illustrated by an arrow 6 and also moved along its length with reference to
5 burner 7 to deposit the soot particles 2 on the mandrel 3 for producing soot porous body 1. During the deposition process, the dopant chemicals for example GeCl4 may also be deposited to form the core of the preform and later the dopant chemicals may be terminated to form clad of the preform. The amount of deposition of the clad region 11 and core region 10 is achieved to
10 have any desired ratio diameter of clad region 11 to the diameter of core region 10.
After completion of deposition, the soot porous body 1 is removed from lathe 5 along with mandrel 3 and handle rod 4, and the mandrel 3 is removed/ detached, during the mandrel removal step, from the soot porous body 1
15 thereby resulting in formation of a hollow cylindrical soot porous body 8 (herein
after referred to as hollow soot porous body) having a centerline 9 therethrough
[Figure 2].
The hollow soot porous body 8 thus formed comprises a core region 10 having a centerline hole 9 and a clad region 11 of the optical fiber preform
20 [Figure 3], and said core region 10 has refractive index greater than that of the clad region 11.
After removal/ detachment of mandrel 3 a centerline 9 is created inside
the soot porous body 1.
Now referring to accompanying Figure 4, the prepared hollow soot porous
25 body 101 is transferred to the sintering furnace 100 in order to achieve dehydration of the hollow soot porous body 101 to form dehydrated hollow soot porous body.
The dehydrated hollow soot porous body is subjected to step of sintering
and collapsing [simultaneously or one after the other] of the centerline 102 to
30 form a solid glass preform 103 [Figure 5] with or without requiring any step of
drilling or grinding or etching of the centerline 9/102 before steps of
consolidation and collapsing.
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Thus, the prepared hollow soot porous body 101 is dehydrated, sintered and collapsed to convert it into solid glass preform 103 [the mother preform].
In a typical embodiment of ACVD method, the hollow soot porous body 101, one end of which is provided with a plug 116 is inserted inside the furnace
5 100 with the help of the handle rod 106. The driving mechanism (not shown) facilitates lowering of the hollow soot porous body 101 into the furnace 100. The furnace 100 comprises a glass muffle tube 110 having a diameter sufficient to accommodate the hollow soot porous body 101 and to adequately provide the environment necessary for dehydration, sintering and collapsing, wherein the
10 sintering and collapsing may either be performed simultaneously or collapsing
step may be performed after sintering step. The muffle tube 110 is suitable for
heating to temperatures necessary for dehydration, sintering and collapsing
process steps with the heating means (not shown) which are suitably fitted to
the sintering furnace 100.
15 The heating means selected may be suitable to create three heat zones
inside the muffle tube 110 over a length. A thermocouple (not shown) provided in the furnace 100 measures the temperature of the hot zones inside the furnace created by the heating means, and the data measurement is fed to the temperature controller (not shown) that controls the temperature inside the
20 muffle tube 110.
The furnace 100 is provided with an inlet port 115 located suitably on the furnace, preferably near the bottom of the muffle tube 110 for supplying desired gases in the furnace. The top end of the muffle tube 110 is suitably closed with the lid 113 to achieve the preferred temperature profile inside the
25 muffle tube 110 and to maintain the same during the dehydration, and simultaneous sintering and collapsing process steps, and to avoid leakage of gases from the muffle tube 110 to the outside environment. A suction port 114 is suitably provided near the top of muffle tube 110 to facilitate evacuation of the gases from the muffle tube 110 as and when required or on completion of
30 the process.
The prepared solid glass preform may optionally be reduced to form a core rod having reduced diameter, which may be overcladded by depositing soot particles to form a soot preform comprising core rod having overclad. The soot
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preform may be sintered in a sintering furnace to form daughter preform. The fiber may also be drawn from the daughter preform.
As described herein above, in accordance with known methods, the process step of collapsing of capillary of a hollow soot porous body, whether
5 carried out simultaneously with sintering step or after performing the sintering step, is carried under a constant vacuum, which has been observed to result in unsymmetrical and incomplete collapsing of the capillary, particularly at its middle portion. The problem of unsymmetrical and incomplete collapsing of the capillary enhances further when the preform having diameter more than about
10 90 mm or weight more than about 9Kg is required to be produced. The preform, whether mother preform or daughter preform, having unsymmetrical and incomplete collapsed capillary [centerline] has been observed to produce a fiber having increased PMD.
Therefore, the present invention aims to overcome above problems and
15 limitations of the prior art.
Accordingly, in one embodiment, the present invention relates to a method for producing optical fiber preform having symmetrically and completely collapsed capillary which is suitable for producing optical fiber having reduced PMD, comprising collapsing the capillary in the hollow soot porous body or
20 sintered glass body under variable vacuum to form optical fiber preform having
symmetrically and completely collapsed capillary.
Accordingly, in another embodiment, the present invention relates to a
method for producing optical fiber having reduced PMD from optical fiber
preform having symmetrically and completely collapsed capillary which is
25 prepared by collapsing the capillary in the hollow soot porous body or sintered
glass body under variable vacuum.
In accordance with present invention, the fiber having reduced PMD may either be drawn at mother preform stage or at daughter preform stage.
It has been observed by the present inventors that if a mother preform is
30 produced in accordance with present invention by collapsing the capillary in the
hollow soot porous body or sintered glass body under variable vacuum, it has
symmetrically and completely collapsed capillary, which has been found
suitable to produce optical fiber having reduced PMD, and has also been found
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suitable to produce a daughter preform which in-turn has been found suitable to produce optical fiber having reduced PMD.
In accordance with present invention, the mother preform having symmetrically and completely collapsed capillary produced in accordance with
5 present invention, preferably has diameter more than about 90 mm or weight more than about 9Kg.
Accordingly, in first preferred embodiment, the present invention relates to a method for producing optical fiber preform having symmetrically and completely collapsed capillary, which is suitable for producing optical fiber
10 having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
having core and clad;
ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
15 iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
20 v) simultaneously sintering and collapsing the dehydrated soot porous body
to collapse the capillary thereby to form mother preform;
characterized in that the simultaneous sintering and collapsing steps on
dehydrated soot porous body to collapse the capillary and to form mother
preform is carried out under variable vacuum.
25 Accordingly, in second preferred embodiment, which is extension of first
embodiment, the present invention relates to a method for producing optical
fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
having core and clad;
30 ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
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iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
v) simultaneously sintering and collapsing the dehydrated soot porous body
5 to collapse the capillary thereby to form mother preform;
vi) drawing the fiber from the mother preform;
characterized in that the simultaneous sintering and collapsing steps on
dehydrated soot porous body to collapse the capillary and to form mother
preform is carried out under variable vacuum.
10 Accordingly, in third preferred embodiment, which is extension of first
embodiment, the present invention relates to a method for producing optical
fiber preform having symmetrically and completely collapsed capillary, which is
suitable for producing optical fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
15 having core and clad;
ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
20 iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
v) simultaneously sintering and collapsing the dehydrated soot porous body
to collapse the capillary thereby to form mother preform;
25 vi) reducing the diameter of the mother preform to form a core rod having
reduced diameter;
vii) overcladding the core rod having reduced diameter to form soot preform
comprising soot porous body having core rod;
viii) sintering the soot preform to form a daughter preform;
30 characterized in that the simultaneous sintering and collapsing steps on dehydrated soot porous body to collapse the capillary and to form mother preform is carried out under variable vacuum.
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Accordingly, in fourth preferred embodiment, which is extension of third embodiment, the present invention relates to a method for producing optical fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
5 having core and clad;
ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
10 iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
v) simultaneously sintering and collapsing the dehydrated soot porous body
to collapse the capillary thereby to form mother preform;
15 vi) reducing the diameter of the mother preform to form a core rod having
reduced diameter;
vii) overcladding the core rod having reduced diameter to form soot preform
comprising soot porous body having core rod;
viii) sintering the soot preform to form a daughter preform;
20 ix) drawing the fiber from the daughter preform;
characterized in that the simultaneous sintering and collapsing steps on dehydrated soot porous body to collapse the capillary and to form mother preform is carried out under variable vacuum.
Accordingly, in fifth preferred embodiment, the present invention relates
25 to a method for producing optical fiber preform having symmetrically and
completely collapsed capillary, which is suitable for producing optical fiber
having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
having core and clad;
30 ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
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iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
v) sintering the dehydrated soot porous body to form sintered glass body;
5 vi) performing collapsing step on sintered glass body to collapse the
capillary thereby to form mother preform; characterized in that the collapsing step on sintered glass body to collapse the capillary and to form mother preform is carried out under variable vacuum.
Accordingly, in sixth preferred embodiment, which is extension of fifth
10 embodiment, the present invention relates to a method for producing optical
fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
having core and clad;
ii) removing the mandrel from the soot porous body to form hollow soot
15 porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
20 porous body;
v) sintering the dehydrated soot porous body to form sintered glass body;
vi) performing collapsing step on sintered glass body to collapse the
capillary thereby to form mother preform;
vii) drawing the fiber from mother preform;
25 characterized in that the collapsing step on sintered glass body to collapse the capillary and to form mother preform is carried out under variable vacuum.
Accordingly, in seventh preferred embodiment, which is extension of fifth
embodiment, the present invention relates to a method for producing optical
fiber preform having symmetrically and completely collapsed capillary, which is
30 suitable for producing optical fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous body
having core and clad;
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ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
5 iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated soot
porous body;
v) sintering the dehydrated soot porous body to form sintered glass body;
vi) performing collapsing step on sintered glass body to collapse the
10 capillary thereby to form mother preform;
vii) reducing the diameter of the mother preform to form a core rod having
reduced diameter;
viii) overcladding the core rod having reduced diameter to form soot preform comprising soot porous body having core rod;
15 ix) sintering the soot preform to form a daughter preform;
characterized in that the collapsing step on sintered glass body to collapse the capillary and to form mother preform is carried out under variable vacuum.
Accordingly, in eighth preferred embodiment, which is extension of seventh embodiment, the present invention relates to a method for producing
20 optical fiber having reduced PMD, comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous
body having core and clad;
ii) removing the mandrel from the soot porous body to form hollow soot
porous body having capillary therethrough;
25 iii) inserting the plug in the bottom end of the capillary of the hollow soot
porous body to close one end thereof;
iv) dehydrating the hollow soot porous body in a suitable environment to
completely remove the moisture in core thereby to form dehydrated
soot porous body;
30 v) sintering the dehydrated soot porous body to form sintered glass
body;
vi) performing collapsing step on sintered glass body to collapse the capillary thereby to form mother preform;
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vii) reducing the diameter of the mother preform to form a core rod
having reduced diameter;
viii) overcladding the core rod having reduced diameter to form soot
preform comprising soot porous body having core rod;
5 ix) sintering the soot preform to form a daughter preform;
x) drawing the fiber from daughter preform;
characterized in that the collapsing step on sintered glass body to collapse the capillary and to form mother preform is carried out under variable vacuum.
As stated herein above, in accordance with present invention, the mother
10 preform having symmetrically and completely collapsed capillary produced in accordance with present invention, preferably has diameter more than about 90 mm or weight more than about 9Kg.
In accordance with present invention, the variable vacuum is varied from bottom end to top end of the soot porous body [referred as body] based on part
15 of the soot porous body or sintered glass body being collapsed.
In accordance with present invention, the vacuum for X length of soot porous body or sintered glass body is different in its bottom part, ramp down part, middle part, ramp up part and top part.
In accordance with preferred embodiment of the present invention, the
20 vacuum inside the body is varied in the range varying from about 130 to about 160 torr while collapsing the bottom portion of the body.
The vacuum inside the body is reduced from a range of about 130 to
about 160 torr in the bottom portion to a range varying from about 170 to
about 190 torr while collapsing ramp down portion of the body.
25 The vacuum inside the body is varied in the range varying from about
170 to about 190 torr while collapsing middle portion of the body.
The vacuum inside the body is increased from a range of about 170 to
about 190 torr in the middle portion to a range varying from about 15 to about
5 torr while collapsing ramp up portion of the body.
30 The vacuum inside the body is varied in the range varying from about 15
to about 5 torr while collapsing top portion of the body.
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In accordance with preferred embodiment of the present invention for X length of soot porous body or sintered glass body the length of bottom part of the body varies from about OX to about 0.36 X.
For X length of soot porous body or sintered glass body the length of
5 ramp down part of the body varies from about 0.36 X to about 0.42 X.
For X length of soot porous body or sintered glass body the length of middle part of the body varies from about 0.42 X to about 0.79 X.
For X length of soot porous body or sintered glass body the length of
ramp up part of the body varies from about 0.79 X to about 0.88 X.
10 For X length of soot porous body or sintered glass body the length of top
part of the body varies from about 0.88 X to IX.
In accordance with particular embodiment of the present invention, for X length of the body,
the vacuum inside the hollow soot porous body or sintered glass body is varied in different portions based on the portion [part] of the soot
15 porous body or sintered glass body being collapsed in following manner:-
The vacuum inside the hollow soot porous body is varied in the range
varying from about 130 to about 160 torr while collapsing the bottom
portion of the soot porous body or sintered glass body;
The vacuum inside the hollow soot porous body is reduced from a range
20 of about 130 to about 160 torr in the bottom portion to a range varying
from about 170 to about 190 torr while collapsing ramp down portion of
the soot porous body or sintered glass body;
The vacuum inside the hollow soot porous body is varied in the range
varying from about 170 to about 190 torr while collapsing middle portion
25 of the soot porous body or sintered glass body;
The vacuum inside the hollow soot porous body is increased from a
range of about 170 to about 190 torr in the middle portion to a range
varying from about 15 to about 5 torr while collapsing ramp up portion of
the soot porous body or sintered glass body;
30 - The vacuum inside the hollow soot porous body is varied in the range
varying from about 15 to about 5 torr while collapsing top portion of the
soot porous body or sintered glass body;
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wherein the length of bottom portion (part) of the soot porous body or sintered glass body varies from about 0.32 X to about 0.36 X, the length of ramp down portion (part) of the soot porous body varies from about 0.36 X to about 0.42 X, the length of middle portion (part) of the soot porous body varies from about
5 0.42 X to about 0.79 X, the length of ramp up portion (part) of the soot porous body varies from about 0.79 X to about 0.88 X, and the length of top portion (part) of the soot porous body varies from about 0.88 X to IX.
In accordance with one of the preferred embodiments of the present invention, the vacuum profile for process step of collapsing, whether
10 simultaneously or preceded by sintering step, is shown in accompanying Figure 6.
In accordance with another preferred embodiment of the present invention, the vacuum profile for process step of collapsing, whether simultaneously or preceded by sintering step, is shown in accompanying Figure
15 7.
In accordance with still another preferred embodiment of the present
invention, the vacuum profile for process step of collapsing, whether
simultaneously or preceded by sintering step, is shown in accompanying Figure
8.
20 In one embodiment, the present invention relates to an optical fiber
preform having symmetrically and completely collapsed capillary when produced in accordance method of the present invention.
In another embodiment, the present invention relates to a method for producing optical fiber having reduced PMD from optical fiber preform which is
25 produced in accordance method of the present invention.
In still another embodiment, the present invention relates to an optical fiber having reduced PMD when produced in accordance with present invention.
It has been observed that optical fiber preform having symmetrically and completely collapsed capillary prepared in accordance with present invention
30 does not show any seeds or bubbles, and hence, no breakage of fiber has been observed during the fiber draw process step.
It has also been observed that optical fiber preform having symmetrically and completely collapsed capillary prepared in accordance with present
18

STER/PA/036
invention shows reduced core ovality in the optical fiber produced from such preform.
It is apparent from the foregoing description that the presently disclosed method has overcome disadvantages, limitations and drawbacks of the prior
5 art.
It may be noted that various terms, for example mandrel, soot porous body, hollow soot porous body, capillary, dehydrated soot porous body, sintered glass body, solid glass preform, core rod having reduced diameter, soot porous body having core rod, core rod, mother preform, soot preform, daughter
10 preform, sintered core rod, bottom portion, ramp down portion, middle portion, ramp up portion etc. as employed herein are merely intended to illustrate the present invention and are not intended to restrict scope of the present invention. It is obvious for the persons skilled in the art that alternative terms may also be employed to describe the present method without deviating from
15 the intended scope of the present invention.
It may also be noted that the presently disclosed method has been described with reference to ACVD method. However, the present method is suitable even for other alternative methods known for producing mother preform and daughter preform.
20
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We Claim :
1. A method for producing optical fiber preform having symmetrically and
completely collapsed capillary which is suitable for producing optical
fiber having reduced PMD, comprising collapsing the capillary in the
5 hollow soot porous body or sintered glass body under variable vacuum.
2. A method for producing optical fiber preform having symmetrically and
completely collapsed capillary comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous
body having core and clad;
10 ii) removing the mandrel from the soot porous body to form hollow
soot porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow
soot porous body to close one end thereof;
iv) dehydrating the hollow soot porous body in a suitable
15 environment to completely remove the moisture in core thereby to
form dehydrated soot porous body;
v) simultaneously sintering and collapsing the dehydrated soot
porous body to collapse the capillary thereby to form mother
preform;
20 characterized in that the simultaneous sintering and collapsing steps on
dehydrated soot porous body to collapse the capillary and to form mother preform are carried out under variable vacuum.
3. A method as claimed in claim 2, further comprising drawing the fiber
from the mother preform produced in process step-v).
25 4. A method as claimed in claim 2, further comprising steps of :-
vi) reducing the diameter of the mother preform produced in process
step-v) to form a core rod having reduced diameter;
vii) overcladding the core rod having reduced diameter to form soot
preform comprising soot porous body having core rod;
30 viii) sintering the soot preform to form a daughter preform.
5. A method as claimed in claim 4, further comprising drawing the fiber from the daughter preform produced in process step-viii).
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STER/PA/036
6. A method for producing optical fiber preform having symmetrically and
completely collapsed capillary comprising steps of:
i) depositing soot particles on the mandrel to prepare a soot porous
body having core and clad;
5 ii) removing the mandrel from the soot porous body to form hollow
soot porous body having capillary therethrough;
iii) inserting the plug in the bottom end of the capillary of the hollow
soot porous body to close one end thereof;
iv) dehydrating the hollow soot porous body in a suitable
10 environment to completely remove the moisture in core thereby to
form dehydrated soot porous body;
v) sintering the dehydrated soot porous body to form sintered glass
body;
vi) performing collapsing step on sintered glass body to collapse the
15 capillary thereby to form mother preform;
characterized in that the collapsing step on sintered glass body to collapse the capillary and to form mother preform is carried out under variable vacuum.
7. A method as claimed in claim 6, further comprising drawing the fiber 20 from the mother preform produced in process step-vi).
8. A method as claimed in claim 6, further comprising steps of :-
vii) reducing the diameter of the mother preform produced in process
step-vi) to form a core rod having reduced diameter;
viii) overcladding the core rod having reduced diameter to form soot
25 preform comprising soot porous body having core rod;
ix) sintering the soot preform to form a daughter preform.
9. A method as claimed in claim 8, further comprising drawing the fiber
from the daughter preform produced in process step-ix).
10. A method as claimed in any one of the preceding claims, wherein said
30 mother preform has diameter more than about 90 mm or weight more
than about 9Kg.
11. A method as claimed in any one of the preceding claims, wherein
vacuum is varied from bottom end to top end of the soot porous body
21

STER/PA/036
based on part of the soot porous body or sintered glass body being collapsed.
12. A method as claimed in claim 11, wherein vacuum for X length of soot
porous body or sintered glass body is different in its bottom part, ramp
5 down part, middle part, ramp up part and top part.
13. A method as claimed in claim 11 or claim 12, wherein vacuum inside the
body is varied in the range varying from about 130 to about 160 torr
while collapsing the bottom portion of the body.
14. A method as claimed in claim 11 or claim 12, wherein vacuum inside the
10 body is reduced from a range of about 130 to about 160 torr in the
bottom portion to a range varying from about 170 to about 190 torr while collapsing ramp down portion of the body.
15. A method as claimed in claim 11 or claim 12, wherein vacuum inside the
body is varied in the range varying from about 170 to about 190 torr
15 while collapsing middle portion of the body.
16. A method as claimed in claim 11 or claim 12, wherein vacuum inside the
body is increased from a range of about 170 to about 190 torr in the
middle portion to a range varying from about 15 to about 5 torr while
collapsing ramp up portion of the body.
20 17. A method as claimed in claim 11 or claim 12, wherein vacuum inside the
body is varied in the range varying from about 15 to about 5 torr while
collapsing top portion of the body. 18. A method as claimed in claim 12, wherein the length of bottom part of
the body varies from about OX to about 0.36 X.
25 19. A method as claimed in claim 12, wherein the length of ramp down part
of the body varies from about 0.36 X to about 0.42 X.
20. A method as claimed in claim 12, wherein the length of middle part of
the body varies from about 0.42 X to about 0.79 X.
21. A method as claimed in claim 12, wherein the length of ramp up part of
30 the body varies from about 0.79 X to about 0.88 X.
22. A method as claimed in claim 12, wherein the length of top part of the
body varies from about 0.88 X to IX.
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23. An optical fiber preform having symmetrically and completely collapsed capillary when produced in accordance with any one of claims 1 to 22.
24. A method for producing optical fiber having reduced PMD from optical fiber preform produced in accordance with any one of the preceding claims 1 to 22.
25. An optical fiber having reduced PMD when produced in accordance with claim 24.
26. A method for producing optical fiber preform substantially as herein described with reference to and as illustrated in the accompanying drawings.
27. A method for producing optical fiber substantially as herein described with reference to and as illustrated in the accompanying drawings.
[Dr. Ramesh Kr. MEHTA]
Patent Attorney for the Applicants
Of Mehta & Mehta Associates
Dated this 13th day of October, 2006
23

Documents:

1712-mum-2006-abstract(1-8-2008).doc

1712-MUM-2006-ABSTRACT(1-8-2008).pdf

1712-mum-2006-abstract-1.jpg

1712-mum-2006-assignment(15-5-2008).pdf

1712-MUM-2006-CLAIMS(1-8-2008).pdf

1712-mum-2006-claims(granted)-(1-8-2008).doc

1712-mum-2006-claims(granted)-(1-8-2008).pdf

1712-mum-2006-claims.pdf

1712-mum-2006-correspondance-other.pdf

1712-MUM-2006-CORRESPONDENCE(1-8-2008).pdf

1712-mum-2006-correspondence(ipo)-(22-9-2008).pdf

1712-mum-2006-correspondence1(20-6-2008).pdf

1712-mum-2006-correspondence2(1-2-2007).pdf

1712-mum-2006-description (complete).pdf

1712-MUM-2006-DESCRIPTION(COMPLETE)-(1-8-2008).pdf

1712-MUM-2006-DRAWING(1-8-2008).pdf

1712-mum-2006-drawings0030.jpg

1712-mum-2006-drawings0031.jpg

1712-mum-2006-drawings0032.jpg

1712-mum-2006-drawings0033.jpg

1712-mum-2006-drawings0034.jpg

1712-mum-2006-drawings0035.jpg

1712-mum-2006-drawings0036.jpg

1712-MUM-2006-FORM 1(1-8-2008).pdf

1712-mum-2006-form 1(16-10-2006).pdf

1712-mum-2006-form 1(20-6-2008).pdf

1712-mum-2006-form 13(15-5-2008).pdf

1712-mum-2006-form 18(6-2-2007).pdf

1712-mum-2006-form 2(1-8-2008).pdf

1712-mum-2006-form 2(granted)-(1-8-2008).doc

1712-mum-2006-form 2(granted)-(1-8-2008).pdf

1712-MUM-2006-FORM 2(TITLE PAGE)-(1-8-2008).pdf

1712-mum-2006-form 26(13-5-2008).pdf

1712-mum-2006-form 3(15-5-2008).pdf

1712-mum-2006-form 3(20-6-2008).pdf

1712-mum-2006-form 5(15-5-2008).pdf

1712-mum-2006-form 5(20-6-2008).pdf

1712-mum-2006-form 9(15-12-2006).pdf

1712-mum-2006-form-2.doc

1712-mum-2006-form1.pdf

1712-mum-2006-form2.pdf

1712-mum-2006-form3.pdf

1712-mum-2006-form5.pdf

1712-mum-2006-other documents(14-5-2008).pdf

abstract1.jpg


Patent Number 226536
Indian Patent Application Number 1712/MUM/2006
PG Journal Number 07/2009
Publication Date 13-Feb-2009
Grant Date 18-Dec-2008
Date of Filing 16-Oct-2006
Name of Patentee STERLITE TECHNOLOGIES LIMITED
Applicant Address E1/E2/E3 MIDC, Waluj, Aurangabad 431136,Maharashtra, INDIA
Inventors:
# Inventor's Name Inventor's Address
1 JIJO PAUL STETLITE TECHNOLOGIES LIMITED., E1/E2/E3, MIDC, Waluj, Aurangabad-431136, Maharashtra,INDIA
2 KAUSHAL GUPTA STERLITE OPTICAL TECHNOLOGIES LTD. E1/E2/E3, MIDC, Waluj, Aurangabad-431136
PCT International Classification Number Co3B37/027,37/03
PCT International Application Number N/A
PCT International Filing date
PCT Conventions:
# PCT Application Number Date of Convention Priority Country
1 NA