Title of Invention

FLUID EJECTION DEVICE AND METHOD OF MANUFACTURING A FLUID EJECTION DEVICE

Abstract A mold (40) configured to be coupled to a fluid ejection head die (30) allow a protective material (38) to be molded around a plurality of contact pads (34) on the die (30) is disclosed. The mold (40) includes a molding surface (43) configured to cover the contact pads (34), wherein the molding surface (43) is configured to support and shape the protective material (38) during molding, and at least one side (45) extending away from the molding surface (43), wherein the side (45) is configured to contain the protective material (38) during molding.
Full Text BACKGROUND OF THE INVENTION
Fluid ejection devices may find uses in a variety of different technologies.
For example, some printing devices, such as printers, copiers and fax machines,
print by ejecting tiny droplets of a printing fluid from an array of fluid ejection
mechanisms onto the printing medium. The fluid ejection mechanisms are
typically formed on a fluid ejection head that is movably coupled to the body of
the printing device. Careful control of the individual fluid ejection mechanisms,
the movement of the fluid ejection head across the printing medium, and the
movement of the medium through the device allow a desired image to be formed
on the medium.
The fluid ejection mechanisms typically are fabricated on a semiconductor
die that forms part of the fluid ejection head, and are controlled by control signals
from off-printhead circuitry. To allow the control signals to reach the fluid ejection
mechanisms, the fluid ejection die includes one or more electrical contacts for
connecting the die to electrical connectors leading to the control circuitry. These
contacts (or contact pads) are typically formed on the same surface of the die as
the openings of the fluid ejection mechanisms.
Due to the proximity of the contact pads to the openings of the fluid
ejection mechanisms on the die surface, it may be possible for fluid to
contaminate the contact pad region of the fluid ejection head die during device
use This may cause electrical shorts to form between adjacent leads, and thus
may degrade printhead performance.
SUMMARY OF THE INVENTION
The present invention provides a mold configured to be coupled to a fluid
ejection head die to allow a protective material to be molded around a plurality of

contact pads on the die. The mold includes a molding surface configured to
cover the contact pads, wherein the molding surface is configured to support and
shape the protective material during molding, and at least one side extending
away from the molding surface, wherein the side is configured to contain the
protective material during molding.
BRIEF DESCRIPTION OF THE DRAWINGS
Fig. 1 is an isometric view of a first embodiment of a fluid ejection device
according to the present invention.
Fig. 2 is an isometric view of a fluid ejection cartridge of the embodiment of
Fig. 1.
Fig. 3 is a partially broken-away isometric view of a protective barrier of
the fluid ejection cartridge of the embodiment of Fig. 1.
Fig. 4 is an isometric view of a mold of the protective barrier of the
embodiment of Fig. 1.
Fig. 5 is a front perspective view of a die of the embodiment of Fig. 1.
Fig. 6 is a magnified, partially-broken away isometric view of the mold and
die of the embodiment of Fig. 1, with the encapsulant omitted for clarity.
Fig. 7 is a sectional view of the mold, die and encapsulant of the
embodiment of Fig. 1.
DETAILED DESCRIPTION
One embodiment of a fluid ejection device according to the present
invention is shown generally at 10 in Fig. 1 as a desktop printer. Fluid ejection
device 10 includes a body 12, and a fluid ejection cartridge 14 operatively
coupled to the body. Cartridge 14 is configured to deposit a fluid onto a medium
16 positioned adjacent to the cartridge. Control circuitry in fluid ejection device
10 controls the movement of cartridge 14 across medium 16, the movement of
the medium under the cartridge, and the firing of individual fluid ejection
mechanisms on the fluid ejection cartridge.
Although shown herein in the context of a printing device, a fluid ejection
device according to the present invention may be used in any number of different
applications. For example, a fluid ejection device according to the present
invention may be used to eject an aerosol, or may find any of a number of uses in

an analytical microfluidic system. Furthermore, while the depicted printing device
takes the form of a desktop printer, a fluid ejection device according to the
present invention may take the form of any other suitable type of printing device,
and may have any other desired size, large- or small-format.
Fig. 2 shows the bottom of cartridge 14 in more detail. Cartridge 14
includes a cartridge body 20 configured to hold a volume of fluid, and a fluid
ejection head 22 coupled to the cartridge body and configured to eject fluid onto
medium 16. An elongate electrical connector 24 is coupled with fluid ejection
head 22 and a side of cartridge body 20 to allow fluid ejection head 22 to be
connected to external control circuitry. Electrical connector 24 may take the form
of a flexible ribbon circuit, and may include a plurality of individual conductive
traces or wires to allow power to be provided separately to each fluid ejection
mechanism. While fluid ejection head 22 is depicted in Fig. 2 as being attached
to cartridge 14, it will be appreciated that a fluid ejection device according to the
present invention may also have a fluid ejection head and a fluid supply
positioned remotely from one another.
If left exposed, the connections between electrical connector 24 and fluid
ejection head 22 may be susceptible to damage from such sources as electrical
shorts caused by fluid contamination or fluid exposure of the leads, and
mechanical damage caused by wiping structures commonly found in fluid ejection
devices. Thus, fluid ejection device 10 also includes a protective barrier, indicated
generally at 26, disposed over selected portions of fluid ejection head 22 to cover
and/or encapsulate the electrical connections between electrical connector 24
and fluid ejection head 22.
Fig. 3 shows the structure of fluid ejection head 22, electrical connector 24
and protective barrier 26 in more detail. Fluid ejection head 22 is formed by
depositing thin films on a die 30, which includes a fluid ejection region 32 having
a plurality of fluid ejection mechanisms (not shown). Die 30 typically takes the
form of a semiconductor substrate, but may be formed from any other suitable
type of substrate as well. A plurality of electrical contacts 34 are formed on the
fluid ejection head 22 and coupled to a plurality of electrical leads 36, which are
coupled to connector 24. Electrical contacts 34 are connected to corresponding

fluid ejection mechanisms, permitting power to be selectively provided to the
individual fluid ejection mechanisms and enabling the controlled ejection of fluid.
Protective barrier 26 may include a plurality of features that combine to
protect contacts 34 and leads 36. For example, in one embodiment, protective
barrier 26 includes a molded encapsulant 38 that extends over electrical contacts
34, and may also include an outer barrier in the form of a preformed mold 40
used to mold encapsulant 38. Encapsulant 38 is configured to encapsulate each
contact 34 and associated leads 36 to electrically insulate each contact and
associated lead from other contacts and leads. This may help to prevent damage
from electrical shorts across the leads in the event of contamination by fluid, and
also from mechanical features such as fluid ejection head wiping stations. Mold
40 also helps to protect contacts 34 and leads 36 from damage from wiping
stations, and may protect encapsulant 38 from corrosion caused by the fluid, if
the encapsulant material is susceptible to corrosion by the fluid.
Encapsulant 38 may be molded around contacts 34 and leads 36 by any
suitable molding process. One example is as follows. First, mold 40 is
positioned over a portion of cartridge 14, as shown in Fig. 2. A bottom inside
portion 43 of moid 40 may serve as a molding surface to contain and shape
encapsulant 38 during the molding process. Bottom inside portion 43 of mold 40
typically includes an opening 44 positioned over fluid ejection region 32 of fluid
ejection head 22 that allows fluid ejected by the fluid ejection mechanisms to
reach the printing medium. Bottom inside portion 43 of mold 40 also may include
a depression 42 formed in the region of the mold that covers contacts 34 and
leads 36 to appropriately space the mold from the contacts and leads. On the
outer surface of the mold, depression 42 is a protrusion over the area of the
contacts 34 and the leads 36. Mold 40 may also include an upturned side portion
45 to help contain encapsulant 38 during the molding process. In one
embodiment, the side portion 45 extends to the cartridge body when the mold 40
is in place on the cartridge.
Mold 40 is placed over the bottom portion of cartridge 14 in such a manner
that a space remains between the bottom of the cartridge and at least part of the
bottom inside portion 43 of the mold. This spacing may be achieved in any

desired manner. For example, the bottom portion 43 of mold 40 may curve away
from the die as it extends away from opening 44. Alternatively, in the depicted
embodiment, mold 40 rests upon a plurality of raised structures situated around
the perimeter of the die, as described in more detail below. In this manner, mold
40 may be quickly and easily positioned on die 30 to have the correct spacing
with respect to the die.
After placing positioning mold 40 over the portion of cartridge 14 as
depicted in Fig. 2, a curable, moldable encapsulant material is added to the mold
and cured to form encapsulant 38. The encapsulant material is typically added in
a large enough quantity to fill the space between mold 40 and die 30 substantially
completely. During the molding process, cartridge 14 is held in an orientation
such that mold 40 and encapsulant 38 are positioned beneath fluid ejection head
22, rotated 180 degrees from that depicted in Fig. 2. This orientation may be
referred to as an "upright" orientation for the purposes of explaining the depicted
embodiment. After encapsulant 38 is cured, preformed mold 40 may be left
adhered to cartridge 22, or may be removed so that encapsulant 38 acts alone as
protective barrier 26.
The molding of encapsulant 38 over contacts 34 and leads 36 offers
various advantages over other methods of forming a protective barrier around the
contacts and leads. For example, a protective barrier could also be formed by
first inverting cartridge 22 to the orientation shown in Fig. 2, and then applying a
curable material over contacts 34 and leads 36 in liquid form via a syringe from
above. However, this method of forming a protective barrier may pose some
difficulties. For example, the rheology of curable material typically must be
carefully controlled. While a low-viscosity curable material may fill the space
between each contact and lead more quickly and thoroughly than a high-viscosity
curable material, the low-viscosity curable material also may tend to run across
the surface of the die too quickly, and thus may contaminate the openings of the
fluid ejection mechanisms. Likewise, the use of a curable material with strong
wetting properties may offer improved coverage of the leads and contacts, but
also may have a higher risk of contaminating the fluid ejection mechanisms.
Additionally, the speed of the application needle, the temperature of the

application process and other environmental factors generally are matched to the
rheology of the curable material, and carefully controlled during the encapsulation
process. These environmental factors tend to change over time, so control of
process may be changed dynamically.
In contrast, in some embodiments, the use of mold 40 allows materials of
a wide variety of viscosities to be easily applied via a low-precision process while
limiting the danger of the encapsulant material contaminating the fluid ejection
mechanisms. When applied via the above-described technique, the encapsulant
material is positioned underneath cartridge 14 during application and curing.
Thus, the encapsulant material is less likely to run and contaminate undesired
portions of fluid ejection head 22 than when the material is applied directly onto
die 30 from above, as gravity tends to hold the encapsulant material within
bottom inside portion 43 of mold 40, whereas gravity tends to encourage the
encapsulant material to wet the surface of the die when applied from above.
Furthermore, as shown in Fig. 7, the inner edge of opening 44 of mold 40 may
upon separators 48 that help to block the encapsulant from running towards the
fluid ejection region 32. These structures are described in more detail below.
Any suitable material may be used to form encapsulant 38. As discussed
above, the use of a curable liquid material with a relatively low viscosity may
allow substantial coverage of all leads 34 and contacts 36 to be achieved more
easily relative to a higher-viscosity encapsulant material. Furthermore, a low-
viscosity material may flow into the spaces between leads 34 and contacts 36
more quickly than a high-viscosity material, and thus may help to decrease the
amount of time to manufacture cartridge 14. The material used to form
encapsulant 38 may also be selected based upon other properties as well. For
example, it may be selected to have sufficient elasticity to avoid fracturing due to
the thermal expansion or contraction of die 30, robustness to withstand repeated
swipes over a fluid ejection head cleaning station commonly found in many fluid
ejection devices, and/or chemical resistance to fluid corrosion. Suitable materials
include, but are not limited to, epoxy materials. Examples of suitable epoxies
include LOCTITE 3563, available from the Loctite Corporation, NAMICS

CHIPCOAT, available from the Namics Corporation, and SIFEL 610, available
from ShinEtsu Silicones of America.
In one embodiment, the material used to form encapsulant 38 may have
any suitable pre-curing viscosity. Suitable pre-curing viscosities include dynamic
viscosities within the range of between approximately 300 and 2500 centipoises,
though viscosities outside of this range may also be used. Likewise, encapsulant
38 may have any suitable dimensions. For example, encapsulant 38 may have a
thickness of 75-100 microns in the region of depression 42. In the regions
adjacent outside of depression 42, encapsulant 38 may have the same thickness
as the height of flow channel separators 48, which are described in more detail
below.
As mentioned above, mold 40 may be left on cartridge 14 after the
encapsulant molding process to form part of protective barrier 26. This may offer
some advantages over removing mold 40 after completing the encapsulant
molding process. For example, because mold 40 is not applied as a curable
viscous material, it may potentially be made from a wider selection of materials
than encapsulant 38, some of which may have more favorable chemical and
mechanical properties than the encapsulant material. One example of a suitable
material for mold 40 is stainless steel. Stainless steel is resistant to corrosion
caused by fluids, fracture from thermal expansion, and mechanical damage
caused by fluid ejection head wiping stations, and is easily formed into the shape
of mold 40. Furthermore, the electrical conductivity of stainless steel does not
affect contacts 34 and leads 36, as the contacts and leads are electrically
insulated from mold 40 by encapsulant 38. Other suitable materials from which
mold 40 may be formed include, but are not limited to, other metals, such as
aluminum, and various polymer materials. Where mold 40 is left on cartridge 14
after the molding process, it may be adhered to the cartridge in any suitable
manner. In some embodiments of the invention, mold 40 is adhered to cartridge
14 by the encapsulant after the encapsulant has cured.
The walls of mold 40 may have any suitable thickness. Where mold 40 is
made from stainless steel foil, an exemplary range of thickness for mold 40 is
between approximately 62 and 87 microns, although foils of thicknesses outside

of this range may also be used. The use of a metal foil to form mold 40 offers the
advantage that the mold may be easily constructed from a single piece of the foil
by a simple forming process.
When mold 40 is left in place after the encapsulant molding process, a
very small area between the edge of the mold and the die may remain unfilled by
encapsulant 38. Where this unfilled area exists, it may be possible for fluid to
contaminate this area. To prevent this space from forming, or to prevent fluid
from contaminating this space, either die 30 or mold 40 may include structure that
permits the encapsulant material to flow into the region between edge 50 of the
mold and the die to form a seal.
One suitable structure for permitting this seal to form is shown in Figs. 5
and 6 as a series of flow channels 46 formed in the surface of die 30. Flow
channels 46 are separated and/or defined by a plurality of flow channel
separators 48 that take the form of raised areas between the flow channels. Flow
channels 46 may act as capillary channels to wick encapsulant into the region of
die 30 underneath the edge of mold 40. Flow channels 46 may be formed on die
30 in any suitable manner, for example, by masking the regions of die 30 where
flow channel separators 48 will be located (as well as other regions of the die that
are not to be etched) with a photo-imageable material, and then etching the
surface of the die. Alternatively, a series of flow channels may be formed in edge
region 50 on bottom inner surface 43 of mold 40, instead of in die 30. Where the
flow channels are formed in the surface of die 30, as in the depicted embodiment,
the flow channel separators may be formed from an oxide layer (or other
electrically insulating layer) formed on the top surface of the die. If desired, an
insulating strip 39 may also be formed along the edge of die 30 to further help to
insulate leads 36 from the bulk of die 30. Insulating strip 39 is located within
encapsulated area, between leads 36 and die 30, and between contacts 34 and
edge of die 30, along one side of die 30. Insulating strip 39 may be formed by
the same etching step as flow channels 46, or may be formed via a separate
processing step.
Flow channels 46 may have any suitable shape. The depicted flow
channels 46 have an elongate shape, and each flow channel connects to

adjacent flow channels at each end. However, the flow channels could also have
a finger-like shape with only one open end, in which case flow channel
separators 48 would connect at one end to fluid ejection region 32 of die 30.
Likewise, flow channels 46 may also have any suitable dimensions. Exemplary
dimensional ranges include a depth of between approximately 20 and 35
microns, a length of between approximately 250 and 500 microns, and a width of
between approximately 30 and 150 microns, though flow channels 46 may also
have dimensions outside of these ranges.
Figs. 6 and 7 show the junction between die 30 and mold 40 in more
detail. The encapsulant is omitted from Fig. 6 for clarity. Referring to Fig. 6,
edge region 50 of mold 40 is configured to rest against the top surfaces of flow
channel separators 48. Because flow channel separators 48 extend above flow
channels 46, edge region 50 does not contact the bottom surfaces of flow
channels 46. Thus, the encapsulant material is free to flow through flow through
channels 46 when added to mold 40. Referring next to Fig. 7, a thin strip 52 of
encapsulant 38 may be formed around edge region 50 from encapsulant material
that flowed through flow channels 46, thus helping to seal any small gaps that
may exist between edge region 50 and the surface of die 30. Selection of an
encapsulant material with suitable wetting properties may help to prevent the
encapsulant from wetting fluid ejection region 32. After curing, encapsulant 38
covers an outer portion of connector 24, and an inner portion of connector 24
between the connector and die 30. In this embodiment, encapsulant 38 isolates
each electrical contact from adjacent electrical contacts. Thus, the largest part of
the outer surface of protective barrier 26 is formed by mold 40, and only thin strip
52 of encapsulant 38 remains exposed where it seals the gap between edge
region 50 and die 30.
Although the present invention has been disclosed in specific
embodiments thereof, the specific embodiments are not to be considered in a
limiting sense, because numerous variations are possible. The subject matter of
the invention includes all novel and nonobvious combinations and
subcombinations of the various elements, features, functions, and/or properties
disclosed herein. The following claims particularly point out certain combinations

and subcombinations regarded as novel and nonobvious. These claims may refer
to "an" element or "a first" element or the equivalent thereof. Such claims should
be understood to include incorporation of one or more such elements, neither
requiring nor excluding two or more such elements. Other combinations and
subcombinations of features, functions, elements, and/or properties may be
claimed through amendment of the present claims or through presentation of new
claims in this or a related application. Such claims, whether broader, narrower,
equal, or different in scope to the original claims, also are regarded as included
within the subject matter of the invention of the present disclosure.

We claim:
1. A fluid ejection device, comprising: a body (20); a die (30) coupled with the body
(20), wherein the die (30) has a fluid ejection means and an electrical contact (34) to the
fluid ejection means; an electrical connector (24) extending along a side of the die (30)
and a side of the body (20), the electrical connector (24) coupled with the electrical
contact (34); and a molded encapsulant (38) covering the electrical contact (34), and at
least a portion of the electrical connector (24), a mold having an edge region, wherein a
plurality of flow channels are formed in the die to receive the molded encapsulant in a
pre-cured state, wherein the flow channels are separated by a plurality of separators, and
wherein the edge region of the mold contacts the separators such that molded encapsulant
flows through the flow channels beneath the edge region of the mold during
manufacturing.
2. The device as claimed in claim 1, comprising a performed mold (40) for molding
the molded encapsulant (38) during manufacturing.
3. The device as claimed in claim 1, wherein the mold (40) having an edge region
(44) on which a plurality of flow channels (46) are formed in the die (30) to receive the
molded encapsulant (38) in a pre-cured state, wherein the flow channels (46) are
separated by a plurality of separators (48), and wherein the edge region (44) of the mold
(40) contacts the separators (48) such that molded encapsulant (38) flows through the
flow channels (46) beneath the edge region (44) of the mold (40) during manufacturing.
4. The device as claimed in claim 3, wherein the flow channels (46) have a length of
between 250 and 550 microns.
5. The device as claimed in claim 3, wherein the flow channels (46) have a width of
between 30 and 150 microns.

6. A print cartridge, comprising: a printhead (22) configured to eject a fluid onto a
printing medium (16), wherein the printhead (22) comprises a die (30) having an
electrical contact (34) and also includes a fluid election region having at least one fluid
ejection mechanism configured to eject the fluid into the printing medium; a connector
(24) coupled to the die (30) having an electrical contact (34); a connector (24) coupled to
the die (30) for electrically connecting the die (30) to off-printhead circuitry, the
connector (24) having a lead (36) that is bonded to the electrical contact (34) on the die
(30); and a preformed barrier (40) coupled with the die (30), wherein the preformed
barrier (40) is configured to protect the lead (36) and the electrical contact (34) from the
fluid, and wherein the preformed barrier includes an opening positioned over the fluid
ejection region to allow fluid ejected by the fluid election mechanism to reach the
printing medium.
7. The print cartridge as claimed in claim 6, wherein the barrier (40) comprises a
raised portion (42) disposed generally adjacent the electrical contact (34) and the lead
(36).
8. A mold (40) configured to be coupled to a fluid ejection head die (30) to allow a
protective material (38) to be molded around a plurality of contact pads (34) on the die
(30), the fluid ejection head die including a fluid ejection mechanism configured to eject
a fluid, the mold (40) comprising: a molding surface (43) configured to cover the contact
pads (34), wherein the molding surface (43) is configured to support and shape the
protective material (38) during molding; at least one side (45) extending away from the
molding surface (43), wherein the side (45) is configured to contain the protective
material (38) during molding; and an opening (44) configured to be positioned over the
fluid ejection mechanism when the mold (40) is coupled to the die (30) so as to allow
fluids ejected from the fluid ejection mechanism to pass through the mold (40).
9. A fluid ejection cartridge (14), comprising : a body (20); a fluid ejection head (22)
operably coupled with the body (20) and including a fluid ejection mechanism configured
to eject a fluid, wherein the fluid ejection head (22) comprises a die (30) having an

electrical contact (34); a connector (24) electrically coupled to the contact (34) on the die
(30); and molded barrier means (38) for protecting the electrical contact (34) and at least
part of the connector (24) from the fluid.
10. A method for protecting an electrical connection of a lead (36) and a contact pad
(34) on a die (30) in a fluid ejection head (22), the fluid ejection head (22) having a fluid
ejection mechanism, the method comprising: coupling a preformed mold (40) with the
die (30) such that the preformed mold (40) is positioned adjacent to and spaced from the
electrical contact (34); and adding a moldable protective materal (38) between the
preformed mold (40) and the electrical contact (34).

A mold (40) configured to be coupled to a fluid ejection head die (30) allow a protective material (38) to be molded around a plurality of contact pads (34) on the die (30) is disclosed. The mold (40) includes a molding surface (43) configured to cover the contact pads (34), wherein the molding surface (43) is configured to support and shape the protective material (38) during molding, and at least one side (45) extending away from the molding surface (43), wherein the side (45) is configured to contain the protective material (38) during molding.

Documents:

759-KOLNP-2005-(22-03-2012)-CORRESPONDENCE.pdf

759-KOLNP-2005-(22-03-2012)-PA-CERTIFIED COPIES.pdf

759-KOLNP-2005-FORM-27.pdf

759-kolnp-2005-granted-abstract.pdf

759-kolnp-2005-granted-assignment.pdf

759-kolnp-2005-granted-claims.pdf

759-kolnp-2005-granted-correspondence.pdf

759-kolnp-2005-granted-description (complete).pdf

759-kolnp-2005-granted-drawings.pdf

759-kolnp-2005-granted-examination report.pdf

759-kolnp-2005-granted-form 1.pdf

759-kolnp-2005-granted-form 13.pdf

759-kolnp-2005-granted-form 2.pdf

759-kolnp-2005-granted-form 3.pdf

759-kolnp-2005-granted-form 5.pdf

759-kolnp-2005-granted-gpa.pdf

759-kolnp-2005-granted-reply to examination report.pdf

759-kolnp-2005-granted-specification.pdf


Patent Number 235019
Indian Patent Application Number 759/KOLNP/2005
PG Journal Number 26/2009
Publication Date 26-Jun-2009
Grant Date 24-Jun-2009
Date of Filing 29-Apr-2005
Name of Patentee HEWLETT-PACKARD COMPANY
Applicant Address 20 BN, 3000, HANOVER STREET, PALO ALTO, CA
Inventors:
# Inventor's Name Inventor's Address
1 ASHOFF CHRIS 6248 SW TRELLIS DRIVE, CORVALLIS, OR 97333
2 REBOA, PAUL, F 2215 NW 29TH STREET, CORVALLIS, OR 97330
3 SMITH GILBERT G 7345 NW MADRONE WAY, CORVALLIS, OR 97330
4 ALTENDORF JOHN M 2375 CHINOOK DR. CORVALLIS, OR 97330
5 BOUCHER WILLIAM R 2040 NE CONIFER BOULEVARD, CORVALLIS, OR 97330
6 ASHOFF CHRIS 6248 SW TRELLIS DRIVE, CORVALLIS, OR 97333
7 REBOA, PAUL, F 2215 NW 29TH STREET, CORVALLIS, OR 97330
8 SMITH GILBERT G 7345 NW MADRONE WAY, CORVALLIS, OR 97330
9 ALTENDORF JOHN M 2375 CHINOOK DR. CORVALLIS, OR 97330
10 BOUCHER WILLIAM R 2040 NE CONIFER BOULEVARD, CORVALLIS, OR 97330
PCT International Classification Number B41J 2/04
PCT International Application Number PCT/US2003/028872
PCT International Filing date 2003-09-12
PCT Conventions:
# PCT Application Number Date of Convention Priority Country
1 10/262,406 2002-09-30 U.S.A.